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Preparation method of titanium-aluminum alloy target

A titanium-aluminum alloy and target technology, which is applied in the field of preparing high-performance targets, can solve the problems of uneven components and low purity of alloy targets, achieve excellent performance and solve the effect of alloy phase separation

Active Publication Date: 2022-01-18
XIANDAO THIN FILM MATERIALS GUANGDONG CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] In view of the deficiencies of the existing technology, a method for preparing a titanium-aluminum alloy target that can effectively solve the problem of uneven composition and low purity of the alloy target is urgently needed in the industry.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0030] The invention provides a method for preparing a titanium-aluminum alloy target, the preparation method comprising the following steps:

[0031] Weighing ingredients: Weigh the titanium raw material and aluminum raw material according to the ratio required by the titanium-aluminum alloy target material, divide the titanium raw material into the first titanium raw material and the second titanium raw material, and divide the aluminum raw material into the first aluminum raw material and the second Aluminum raw material.

[0032] According to the difference in melting point and density between two metal elements, titanium and aluminum, in order to avoid incomplete smelting or component segregation, the method adopts a step-by-step smelting method for smelting.

[0033] Primary smelting: the first titanium raw material and the first aluminum raw material are placed in a water-cooled copper crucible, vacuumized, then powered and heated, and smelted to obtain the first titani...

Embodiment 1

[0048] (1) Weighing ingredients: Weigh the titanium raw material and the aluminum raw material according to the mass ratio of the titanium raw material and the aluminum raw material as 16:9, divide the titanium raw material into the first titanium raw material and the second titanium raw material, and divide the aluminum raw material into the first titanium raw material Aluminum raw materials and second aluminum raw materials, wherein, the first titanium raw material accounts for 50wt% of the total amount of titanium raw materials, the second titanium raw material accounts for 50wt% of the total amount of titanium raw materials, the first aluminum raw material accounts for 50wt% of the total amount of aluminum raw materials, and the second The secondary aluminum raw material accounts for 50wt% of the total aluminum raw material;

[0049] (2) Primary smelting: put the first titanium raw material and the first aluminum raw material in a water-cooled copper crucible, place the fir...

Embodiment 2

[0058] (1) Weighing ingredients: Weigh the titanium raw material and the aluminum raw material according to the mass ratio of the titanium raw material and the aluminum raw material as 32:9, divide the titanium raw material into the first titanium raw material and the second titanium raw material, and divide the aluminum raw material into the first titanium raw material Aluminum raw materials and second aluminum raw materials, wherein, the first titanium raw material accounts for 60wt% of the total amount of titanium raw materials, the second titanium raw material accounts for 40wt% of the total amount of titanium raw materials, the first aluminum raw material accounts for 40wt% of the total amount of aluminum raw materials, and the second The secondary aluminum raw material accounts for 60wt% of the total aluminum raw material;

[0059] (2) Primary smelting: put the first titanium raw material and the first aluminum raw material in a water-cooled copper crucible, place the fir...

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Abstract

The invention discloses a method for preparing a titanium-aluminum alloy target, which includes: weighing titanium raw materials and aluminum raw materials, dividing the titanium raw materials into first titanium raw materials and second titanium raw materials, and dividing the aluminum raw materials into first aluminum raw materials and second titanium raw materials. The second aluminum raw material; the first titanium raw material and the first aluminum raw material are placed in a water-cooled copper crucible and smelted to obtain the first melt; the first melt is cooled to obtain the first ingot; the first ingot is placed in the water-cooled copper crucible bottom, and add a second titanium raw material and a second aluminum raw material for smelting to obtain a second melt; cool the second melt to obtain a second ingot; heat the second ingot until it is completely melted, refine it, and quickly cast it to obtain a target. The target blank is packaged, degassed, hot isostatically pressed, and finally sintered to obtain a sintered body; the sintered body is taken out of the package and then machined to obtain a titanium-aluminum alloy target. The invention adopts a step-by-step smelting method, which can solve the technical problems such as a large number of shrinkage cavities, porosity and other defects in the preparation of titanium-aluminum alloy target materials in the prior art.

Description

Technical field [0001] The invention relates to the technical field of preparing high-performance target materials, and in particular to a method for preparing titanium-aluminum alloy targets. Background technique [0002] Titanium-aluminum alloy targets are mainly used in the tool coating industry. Targets are generally manufactured by smelting, hot pressing or isostatic pressing. Among them, smelted targets have better alloying, while hot-pressed targets have lower costs but low density. , Hot isostatic pressing targets have the advantage of high density and can be mass produced. During the use of the target, reactive sputtering is generally carried out in an environment such as nitrogen or acetylene to form a coating. Titanium aluminum N, CrN, and titanium aluminum CrN are new hard coating materials developed in recent years. Titanium-aluminum N-coated blades have been commercialized. It has good chemical stability and anti-oxidation wear performance. When using it to ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C14/00C22C1/02C22C1/04B22F3/16
CPCC22C14/00C22C1/02C22C1/0458B22F3/16
Inventor 蔡新志童培云朱刘冉成义王慧康
Owner XIANDAO THIN FILM MATERIALS GUANGDONG CO LTD
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