Two-dimensional cadmium hydroxide material, preparation method, growth template and application

A technology of cadmium hydroxide and cadmium salt, which is applied in chemical instruments and methods, nanotechnology for materials and surface science, cadmium compounds, etc. Cost, simple effect of preparation method

Active Publication Date: 2021-06-04
SHENZHEN INST OF ADVANCED TECH CHINESE ACAD OF SCI
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The prepared self-supporting hydroxide film of the above scheme is 150∼800nm, which cannot meet the requirements of electronic devices and sensors

Method used

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  • Two-dimensional cadmium hydroxide material, preparation method, growth template and application
  • Two-dimensional cadmium hydroxide material, preparation method, growth template and application
  • Two-dimensional cadmium hydroxide material, preparation method, growth template and application

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preparation example Construction

[0072] Embodiment 2 of the present invention discloses a preparation method of a two-dimensional cadmium hydroxide material, such as figure 1 shown, including the following steps:

[0073] S1. prepare organic cadmium salt solution;

[0074] S2. Provide a two-phase system solvent, the upper layer of the two-phase system solvent is a non-polar solvent layer, and the lower layer is a polar solvent layer;

[0075]S3. The organic cadmium salt solution gathers at the interface between the non-polar solvent and the polar solvent;

[0076] S4. Evaporating the non-polar solvent layer located on the upper layer, so that the organic cadmium salt at the interface gathers to form a film as the volume of the non-polar solvent decreases, and floats on the liquid surface of the polar solvent layer;

[0077] S5. Inject the basic polar solvent into the polar solvent in the lower layer to form a two-dimensional cadmium hydroxide bilayer film; when the basic polar solvent is added, the temperat...

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Abstract

The invention relates to a two-dimensional cadmium hydroxide material, a preparation method, a growth template and application. The two-dimensional cadmium hydroxide material is a cadmium hydroxide-fatty acid two-dimensional double-layer film, and the thickness of the film is smaller than or equal to 5 nm. The preparation method comprises the following steps: an organic cadmium salt solution is prepared; a two-phase system solvent is provided, the upper layer of the two-phase system solvent is a non-polar solvent layer, and the lower layer of the two-phase system solvent is a polar solvent layer; the organic cadmium salt solution is gathered at the interface of the non-polar solvent and the polar solvent; the non-polar solvent layer located on the upper layer is evaporated, so that the organic cadmium salt is gathered into a film along with the volume of the non-polar solvent, and floats on the liquid surface of the polar solvent layer; and the alkaline polar solvent is injected into the polar solvent at the temperature of less than 150 DEG C to generate a two-dimensional cadmium hydroxide double-layer film. The cadmium hydroxide-fatty acid two-dimensional double-layer film can be applied to growth templates for growing two-dimensional cadmium sulfide and cadmium selenide and electronic devices; and the preparation method is simple, efficient and easy for industrial production.

Description

technical field [0001] The invention relates to a two-dimensional cadmium hydroxide material, especially a two-dimensional cadmium hydroxide material, a preparation method, a growth template and application. Background technique [0002] Since the discovery of graphene, two-dimensional materials have attracted much attention due to their unique electrical, optical, magnetic and mechanical properties and their potential applications in the construction of nanodevices. Exploring large-area, single-layer or few-layer two-dimensional materials has been a research hotspot. Relevant researchers and technicians have made many attempts in the preparation of two-dimensional materials, among which chemical vapor deposition (CVD), mechanical exfoliation, hydrothermal method, etc. are commonly used two-dimensional material preparation methods. However, mechanical exfoliation and hydrothermal methods cannot prepare large-area two-dimensional materials; and although chemical vapor deposi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01G11/00B82Y30/00
CPCC01G11/00B82Y30/00C01P2004/04C01P2004/03C01P2004/02C01P2002/84C01P2004/20C01P2004/64
Inventor 吴昊张阳阳李江宇
Owner SHENZHEN INST OF ADVANCED TECH CHINESE ACAD OF SCI
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