Novel semiconductor single crystal wafer dislocation density detection corrosion tool and method
A chip and tooling technology, which is applied in the corrosion field of silicon carbide wafers, can solve the problems that the corrosion safety and stability have not been significantly improved.
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Embodiment 1
[0058] Segmental lipping preheating and cooling method
[0059] Using the lift rod according to the decrease in divisions and lifting, only the wafer clamp in the tool is used.
[0060] Specific steps are as follows:
[0061] Step 1: Analyze 1.5 kgKOH to the melt to melt, keep the molten liquid temperature of about 505 ° C;
[0062] Step 2: The wafer clamp is mounted to the pullement rod, and the low heat is lowered at a height of the near liquid surface;
[0063] Step 3: The lower clamp is to enter the liquid surface at the bottom, and the wafer remains above the liquid surface, preheating for 2min;
[0064] Step 4: Continue drop to the wafer to immerse corrosion fluid, corrode 4.5 min;
[0065] Step 5: Corrosion is completed, lift the clamp to the distance liquid surface 2 cm, maintained 3.5 min;
[0066] Step 6: Rapidity to 10cm from the liquid level, cool 2min;
[0067] Step 7: Horizontal moving fixture to the cooling station, cool to 147 ° C;
[0068] Step 8: Place the fixtur...
Embodiment 2
[0072] Continuous liping and cooling method
[0073] Corrosion and improvement in the stepper motor, only the wafer clamp in the tooling.
[0074] Specific steps are as follows:
[0075] Step 1: Analyze 1.5 kgkoH to analyze the purifier to melt, keep the molten liquid temperature of about 511 ° C;
[0076] Step 2: The wafer clamp is mounted to the pull rod, and the low heat is lowered at a height of the near liquid surface;
[0077] Step 3: Control the stepper motor speed of 2.5mm / s, a falling fixture, and a preheating is 2min;
[0078] Step 4: Continuously drop the wafer and immersed in the corrosive liquid, corroded 4 min;
[0079] Step 5: Corrosion is completed, which increases the jig to 15cm from the liquid level at 3 mm / s.
[0080] Step 6: Horizontal moving fixture to the cooling station, cool to 152 ° C;
[0081] Step 7: Place the fixture and the wafer in a 90 ° C water bath and soak for 3 min.
[0082] Step 8: Take out the wafer, remove the deionized water, dry, dry, o...
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