Delayed curing UV adhesive and preparation method thereof

A curing type, aluminum sheet technology, applied in the direction of adhesives, epoxy resin adhesives, non-polymer organic compound adhesives, etc., can solve the problems of insufficient exposure of transparent substrates, affecting the performance of optical products, and complex application scenarios. Achieve good toughness, small curing shrinkage, and promote the effect of dark reaction

Pending Publication Date: 2021-08-17
浙江国能科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] However, in some optical devices, the application scenarios are more complicated. For example, the transparent substrate of the adhered device cannot be fully exposed, or it is required to be in a certain light protection scene, so it cannot be exposed to ultraviolet light for a long time, otherwise it will affect the optical product. Other properties; or some optical devices can only be used for positioning in the early stage of the production process, so as to facilitate the subsequent production of other processes, otherwise the rework will be very difficult or cause the product to be scrapped, or even the bonded part is completely opaque materials, etc.
For the above application scenarios with difficult process requirements, the existing UV adhesive technology can hardly solve these difficulties and pain points because it can be completely cured by one irradiation and requires at least one side of transparent material.

Method used

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  • Delayed curing UV adhesive and preparation method thereof
  • Delayed curing UV adhesive and preparation method thereof
  • Delayed curing UV adhesive and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Based on 100 parts by weight proportioning, prepare the UV glue composition according to the following formula:

[0025] components Name of raw material provider Mass % Prepolymer 6148J75 Changxing Chemical 40 epoxy resin 2021P Nantong Synasia New Materials Co., Ltd. 20 active monomer 2-HEMA BASF 30 Auxiliary 2-28 Nantong Synasia New Materials Co., Ltd. 1.67 coupling agent 171 Wacker 1.67 antioxidant ADK STAB 517 Japan Adico 1.67 Initiator A 1173 Huatai Chemical 1.67 Initiator B 101 Guangyi Chemical 3.5

[0026] Preparation:

[0027] Add the prepolymer, epoxy resin, active monomer, auxiliary agent, silane coupling agent, antioxidant, photoinitiator, etc. into the three-dimensional mixer in sequence, with a total of 100g, and keep the temperature not higher than 50 degree, select 1000 rev / min, under the condition of avoiding light, disperse and mix for 10 minutes, and then filter...

Embodiment 2

[0049] Prepare UV glue composition according to following formula (preparation method and test method are identical with embodiment one):

[0050]

[0051] The various aspects performance of the UV glue that embodiment two obtains is as follows:

[0052]

Embodiment 3

[0054] Prepare UV glue composition according to following formula (preparation method and test method are identical with embodiment one):

[0055]

[0056] The various aspects performance of the UV glue that embodiment three obtains is as follows:

[0057]

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Abstract

The invention discloses a delayed curing UV adhesive for bonding transparent media such as glass and glass, glass and aluminum sheets and non-transparent media such as aluminum sheets and aluminum sheets and aluminum sheets and plastic and a preparation method of the delayed curing UV adhesive, and relates to the technical field of glue preparation. The UV adhesive comprises the following main components: a prepolymer accounting for 40-65% of the weight of the UV adhesive, epoxy resin accounting for 20-40% of the weight of the UV adhesive, an active monomer accounting for 15-25% of the weight of the UV adhesive, an auxiliary agent accounting for 1-3% of the weight of the UV adhesive, a silane coupling agent accounting for 0.5-2.0% of the weight of the UV adhesive, an antioxidant accounting for 0.5-2.0% of the weight of the UV adhesive, a photoinitiator A accounting for 0.5-2% of the weight of the UV adhesive, and a photoinitiator B accounting for 0.5-5% of the weight of the UV adhesive. The delayed curing optical UV adhesive is very suitable for adhesion of non-transparent media, and the characteristic that the existing commercially available UV adhesive can only adhere to an adherend and at least one surface of the adherend is a transparent medium is changed.

Description

technical field [0001] The present invention relates to the technical field of glue preparation, more specifically, it relates to transparent media such as glass and glass, glass and aluminum flakes, and non-transparent media such as aluminum flakes and aluminum flakes, aluminum flakes and plastics, etc. Optical UV glue and its preparation method. Background technique [0002] Ultraviolet light curing adhesive technology, also known as UV glue technology, has developed rapidly in the past ten years due to its high efficiency, energy saving, environmental protection, convenient operation and many other advantages, and its application fields have gradually expanded. At present, it has covered electronics, microelectronics, Aerospace, automotive, industrial and civil and many other fields. [0003] When UV glue is cured, free radicals are generated due to the need for light penetration, which then initiates polymerization. Therefore, its application often requires at least one...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J163/00C09J4/06C09J4/02
CPCC09J163/00C09J4/06
Inventor 宋志国胡云睿吕本荣
Owner 浙江国能科技有限公司
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