A Clay Mineral Oriented Sheet Atomization Treatment Device and Treatment Method

A clay mineral and processing device technology, applied in the field of atomization processing devices, can solve problems such as XRD analysis errors, achieve the effects of reducing sample errors, improving experimental testing efficiency, and protecting health and safety

Active Publication Date: 2022-01-28
INST OF GEOLOGY & GEOPHYSICS CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] In order to overcome the above technical problems in the prior art, the present invention designs a set of ethylene glycol atomization device, which effectively solves the problem of XRD analysis error caused by different expansive clay content and drying time difference

Method used

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  • A Clay Mineral Oriented Sheet Atomization Treatment Device and Treatment Method
  • A Clay Mineral Oriented Sheet Atomization Treatment Device and Treatment Method
  • A Clay Mineral Oriented Sheet Atomization Treatment Device and Treatment Method

Examples

Experimental program
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Effect test

Embodiment 1

[0094] Such as Figure 1-Figure 3 As shown, a clay mineral directional sheet atomization treatment device, the device as a whole adopts a full set of corrosion-resistant materials, including an atomization box 22, which is a fully airtight sealed box, and an atomizer 16 is arranged outside the atomization box 22 The atomization box 16 is provided with a sensor and a spray assembly. The sensor includes an air pressure sensor 1 and a temperature sensor 3. The air pressure sensor 1 and the temperature sensor 3 are arranged on the upper part of the atomization box 22 for controlling the air pressure and temperature in the atomization box. . One end of the spray assembly is horizontally arranged in the atomization box 16, and the other end extends to the outside of the atomization box 16. The spray assembly can change the position of the spray through the servo motor and the moving assembly to realize horizontal and vertical movement of the spray in the same plane. Shower, the bot...

Embodiment 2

[0112] A method for atomizing the directional sheet of clay minerals, which is carried out using the processing equipment in Example 1, specifically comprising the following steps:

[0113] (1), first check the airtightness of the atomization treatment device: insert the empty drawer 4 directly into the atomization box 22, close the conduit valve 2 and the air release valve 20, turn on the vacuum pump 9, and open the exhaust pipe valve 13, do not need to open Cooling water, pump the inside of the atomization box 22 into a negative pressure, then close the exhaust pipe valve 13, turn off the vacuum pump 9, observe the reading of the air pressure sensor 1, the vacuum degree in the atomization box 22 remains unchanged, indicating that the airtightness is normal, then you can Normal use;

[0114](2), carry out organic solvent ethylene glycol, glycerin saturation treatment: put the oriented sheet 17 that is coated with clay mineral in the drawer 4, insert the drawer 4 into the atom...

Embodiment 3

[0121] A kind of atomization treatment method of clay mineral orientation sheet, and embodiment 1 is similar, and difference is, as Figure 4 with Figure 5 As shown, a sealing block 43 is fixedly connected to the inner side of the sealing plate 42, the sealing block 43 is a right-angled triangle sealing block, and the outer surface of the sealing block 43 is inclined. Corresponding sockets are also provided at the corresponding positions of the sealing block 43 and the sealing plate 42 to facilitate the insertion of the cover plate. A movable baffle assembly 23 is provided on the inner side of the box wall of the atomization box 22 located on the upper part of the sealing block 43 . The movable baffle assembly includes an inner baffle 231 and an outer baffle 232, and the inner baffle 231 and the outer baffle 232 are arranged separately. The inner layer baffle plate 231 and the outer layer baffle plate 232 are adjacent and arranged in parallel. The inner layer baffle plate 2...

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Abstract

The present invention provides a clay mineral directional sheet atomization treatment device and treatment method. A sensor and a spray assembly are arranged in the atomization box. One end of the spray assembly is horizontally arranged in the atomization box, and the other end extends to the outside of the atomization box. , The spraying component can change the position of the spraying through the servo motor and the moving component to realize the horizontal and vertical movement of the spraying, and the bottom of the atomization box is equipped with a heating device. It effectively solves the problem of XRD analysis error caused by different expansive clay content and drying time. At the same time, the non-contact ethylene glycol saturation treatment process is adopted to achieve the greatest protection for the personal health of the experimenters. The non-contact saturation treatment process prevents the experimenters from contacting toxic reagents and protects health and safety. The invention can process 200 samples at one time, greatly improving the efficiency of experimental testing; ensuring that each sample to be tested has the same organic saturation degree, and reducing the error of different samples.

Description

technical field [0001] The invention belongs to an atomization treatment device, in particular to an atomization treatment device and a treatment method for a clay mineral oriented sheet. Background technique [0002] At present, in the identification of clay minerals, X-ray diffractometer (XRD for short) testing and identification of characteristic diffraction peaks in XRD diffraction patterns are the most widely used identification methods. Since different minerals may have the same diffraction peaks, the preparation of clay mineral oriented slices under different pretreatment conditions is a key step in identification. In samples containing expansive clay minerals (such as montmorillonite, vermiculite, etc.): filling organic molecules into the expansive mineral lattice to increase the lattice spacing is the difference between Diffraction peaks for expansive minerals (montmorillonite, vermiculite) and non-expandable minerals (chlorite) key method. [0003] As a kind of ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N23/20008G01N23/207
CPCG01N23/20008G01N23/207
Inventor 胡彬张春霞张晓燕
Owner INST OF GEOLOGY & GEOPHYSICS CHINESE ACAD OF SCI
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