Continuous casting tundish magnesia-calcium dry vibrating material and preparation method thereof
A dry vibrating material, coated with magnesium and calcium, is used in the field of refractory materials to reduce pollution, improve slag resistance, and improve erosion resistance.
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[0034] A method for preparing a continuous casting tundish magnesium-calcium dry vibration material, specifically comprising:
[0035] 1) Crushing the waste magnesia-calcium-carbon bricks in a crusher, sieving them into raw materials of 0<grain size≤1mm, 1mm<grain size≤3mm, 3mm<grain size≤5mm;
[0036] 2) The crushed magnesia-calcium-carbon waste brick particles are dried in a rotary kiln for 3-5 minutes after iron removal, and the drying temperature is 400°C-450°C.
[0037] 3) crush 91 magnesia in a crusher, and sieve it into raw materials of 1mm<grain size≤3mm, 3mm<grain size≤5mm;
[0038] 4) Crushing the 95 mid-grade magnesia in a crusher, and sieving it into raw materials with a particle size of 0<1mm and below 200 mesh;
[0039] 5) weighing the raw materials according to the proportioning ratio for subsequent use;
[0040] 6) Mixing
[0041] First add 5-3mm, 3-1mm, 1-0mm raw materials and dry mix for 3-5 minutes, then add binder and red clay, and mix for another 3-5 mi...
Embodiment 1
[0049] The scanning electron microscope figure of embodiment 1 is shown in figure 2 , the energy spectrum of the scanning electron microscope is shown in image 3 .
Embodiment 4
[0050] The scanning electron microscope figure of embodiment 4 is shown in Figure 4 , the energy spectrum of the scanning electron microscope is shown in Figure 5 .
[0051] It can be seen from the electron microscope scanning images of the above two examples that the microstructure of Example 1 has very uniform particles, and its main elements are Mg, Al, Si, Ca, Fe, O. The microstructure of Example 4 after adding magnesium-calcium carbon shows that the particles are relatively uniform, and no new substances are formed. The proportion of Ca increases due to the addition of magnesium-calcium carbon, and the rest does not change much.
[0052] It can be seen from the data that Example 4 is better than Example 1 in bulk density and flexural tests at 1500°C, and in the slag resistance test, because Example 4 contains CaO, it can purify molten steel and enhance its resistance to slag. Slag capacity, so comprehensive consideration embodiment 4 is better than embodiment 1.
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