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Low-temperature QPQ treatment process for 316L stainless steel workpiece

A treatment process, stainless steel technology, applied in the direction of metal material coating process, coating, solid-state diffusion coating, etc., can solve the problem of reduced corrosion resistance, achieve the effect of improving wear resistance and avoiding secondary tempering

Pending Publication Date: 2022-01-07
CHENGDU TOOL RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to provide a low-temperature QPQ treatment process for 316L stainless steel workpieces, solve the problem that the corrosion resistance of 316L stainless steel materials will be reduced after conventional QPQ treatment, and at the same time improve the wear resistance and hardness of 316L stainless steel workpieces

Method used

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  • Low-temperature QPQ treatment process for 316L stainless steel workpiece
  • Low-temperature QPQ treatment process for 316L stainless steel workpiece
  • Low-temperature QPQ treatment process for 316L stainless steel workpiece

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A kind of 316L stainless steel workpiece low-temperature QPQ processing technology, it is characterized in that carrying out according to the following flow process:

[0022] Step 1, cleaning: Soak the 316L stainless steel workpiece in the stain-removing oil for 5 minutes. The oil stain on the surface of the workpiece is completely removed as the standard. When the oil stain on the surface of the workpiece is extremely serious, the soaking time can be extended appropriately; A 14kw ultrasonic cleaning machine cleans the workpiece at 65°C for 30 minutes, then takes out the workpiece and rinses it twice with clean water, with a single rinse time of 3 minutes. Try to ensure that there is no residue of decontamination oil on the surface of the workpiece.

[0023] Step 2, preheating: Use compressed air to blow off as much residual water as possible on the surface of the cleaned 316L stainless steel workpiece, then place the workpiece in a preheating furnace at 350°C for 30 mi...

Embodiment 2

[0031] The difference between embodiment 2 and embodiment 1 is:

[0032] Step 1, cleaning: Soak the 316L stainless steel workpiece in stain-removing oil for 2 minutes, then use an ultrasonic cleaning machine with an ultrasonic frequency of 25KHZ and an ultrasonic power of 14kw to clean the workpiece at 70°C for 20 minutes, then take out the workpiece and rinse it twice with clean water. The rinse time is 2 minutes.

[0033] Step 2, preheating: After blowing off as much water as possible on the surface of the cleaned 316L stainless steel workpiece, place the workpiece in a preheating furnace at 380°C for 45 minutes.

[0034] Step 3, Nitriding: Then add the nitride salt for low-temperature QPQ into the nitriding furnace, heat the nitride salt in the nitriding furnace to its molten liquid state, and then put the preheated workpiece into the nitriding furnace , the furnace temperature was maintained at 425 ° C for 600 min for nitriding. In the molten state, the nitride salt is c...

Embodiment 3

[0041] The difference between embodiment 3 and embodiment 1 and embodiment 2 is:

[0042] Step 1, cleaning: Soak the 316L stainless steel workpiece in stain-removing oil for 3 minutes, then use an ultrasonic cleaning machine with an ultrasonic frequency of 25KHZ and an ultrasonic power of 14kw to clean the workpiece at 60°C for 15 minutes, then take out the workpiece and rinse it twice with clean water. The rinse time is 4 minutes.

[0043] Step 2, preheating: After blowing off as much water as possible on the surface of the cleaned 316L stainless steel workpiece, place the workpiece in a preheating furnace at 355°C for 60 minutes.

[0044] Step 3, Nitriding: Then add the nitride salt for low-temperature QPQ into the nitriding furnace, heat the nitride salt in the nitriding furnace to its molten liquid state, and then put the preheated workpiece into the nitriding furnace , the furnace temperature was maintained at 430 ° C for 480 min for nitriding. In the molten state, the ...

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Abstract

The invention discloses a low-temperature QPQ treatment process for a 316L stainless steel workpiece, and relates to the technical field of metal surface heat treatment. According to the key point of the technical scheme, the low-temperature QPQ treatment process comprises the steps that molten liquid-state nitriding salt is arranged in a nitriding furnace, then a pretreated workpiece is put into the nitriding furnace, the furnace temperature is kept at 430 + / -5 DEG C, and nitriding is carried out for 480-720 minutes; and a molten liquid-state oxidizing salt is arranged in an oxidizing furnace, then the workpiece processed in the previous step is put into the oxidizing furnace at the temperature of 380 DEG C + / -5 DEG C to be oxidized for 15-30 minutes, and after oxidation is completed, the workpiece is subjected to prognosis treatment. The surface hardness, wear resistance and fatigue resistance of the 316L stainless steel workpiece can be obviously improved, and the corrosion resistance of the workpiece is not reduced.

Description

technical field [0001] The invention belongs to the technical field of metal surface heat treatment, and relates to a low-temperature QPQ treatment process for 316L stainless steel workpieces. Background technique [0002] QPQ treatment technology is a composite technology of liquid nitriding and liquid oxygenation technology, because its raw materials do not contain any heavy metal elements, so it is also an environmentally friendly technology. The principle is to use the active nitrogen atoms produced by the decomposition of cyanate to penetrate into the workpiece, forming a layer of high nitrogen concentration nitriding layer on the surface of the workpiece, thereby improving the surface hardness, wear resistance and fatigue resistance of 316L stainless steel workpieces, so QPQ Technology has been widely used in production practice. [0003] Due to the low carbon content, austenitic stainless steel cannot be strengthened through phase transformation. Although the convent...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C8/50C23C8/58C23C8/02C23C8/80
CPCC23C8/50C23C8/58C23C8/02C23C8/80
Inventor 汪辉谢明强吴少旭王强代燕芹文灿李皓荣
Owner CHENGDU TOOL RES INST