Efficient and accurate daily porcelain 3d soft silicone transfer ink and its application
A soft silicone, daily-use technology, used in inks, applications, home appliances, etc., to achieve clear edges, high precision, and accurate colors
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Embodiment 1
[0035] The sodium polyacrylate-aluminum sol composite solution A was prepared by the following method: in a stirring reactor, add sodium polyacrylate to normal temperature water, beat until it becomes a glue, add aluminum isopropoxide and stir for 4 days to generate a transparent light milky white glue , heated to 80-85°C for 1 h under reduced pressure and distilled for 1 h until sampling to detect that there was no residual isopropanol and the concentration of aluminum-containing sol was 12% in terms of alumina, and cooled to room temperature to obtain sodium polyacrylate-aluminum sol composite solution A. The mass ratio of ingredients is water, sodium polyacrylate, and aluminum isopropoxide=120:1.3:30. The sodium polyacrylate used was XM-500 from Zhejiang Chunan Xumedia Biotechnology Co., Ltd., with a degree of polymerization of 1200-1300. The purity of aluminum isopropoxide is over 99.9%.
[0036] The obtained sodium polyacrylate-aluminum sol composite solution A was trans...
Embodiment 2
[0038] The sodium polyacrylate-aluminum sol composite solution B was basically prepared according to the method of Example 1: in the same stirring reactor, sodium polyacrylate was added to normal temperature water, beating until it became a glue solution, and aluminum isopropoxide was added to stir and react for 5 days, and a transparent solution was formed. The light milky white glue solution was heated to 80-85°C under reduced pressure for 1 h until no isopropanol remained and the concentration of aluminum-containing sol was 15% based on alumina, and cooled to room temperature to obtain sodium polyacrylate-aluminum sol composite solution B. The mass ratio of ingredients is proportioned according to water, sodium polyacrylate, aluminum isopropoxide=120:2:50.
[0039] The obtained sodium polyacrylate-aluminum sol composite solution B was transparent and light milky white, with a pH of 8.3, and a clear light path was visible when irradiated by thin beams of light, and the averag...
Embodiment 3
[0045] The thermosetting phenolic resin C was prepared by the following method: in a stirring reactor, 37m% of the commercial aqueous solution of formaldehyde was calculated as formaldehyde, phenol and borax decahydrate were calculated as anhydrous, and the proportion of substances was 1.6:1:0.015. Formaldehyde aqueous solution and phenol are mixed, beat, heat up to 70°C and stir for 15min, add dropwise saturated aqueous solution of borax, heat up to 85-90°C and keep the temperature for 3h, then distill under reduced pressure at 85-90°C for 1.5h to Sampling to detect no formaldehyde, no residual phenol and about 35m% of water, and cooled to room temperature to obtain heat-cured phenolic resin C.
[0046] The obtained heat-cured phenolic resin C was transparent and light brownish red; it was stable and had no visible change for 3 months when stored at room temperature in a closed light-shielding manner.
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