Arylamine organic compound, mixture, composition and organic electronic device
A technology of organic electronic devices and organic compounds, which is applied in the fields of aromatic amine organic compounds, compositions and organic electronic devices and mixtures, which can solve problems such as insufficient device life, unbalanced electron transmission, and device holes, and improve luminous efficiency and lifetime, and the effect of good hole transport performance
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Embodiment 1
[0105] The synthesis of embodiment 1 compound 1
[0106]
[0107] Synthesis of Intermediate 1-3: Compound 1-1 (20mmol), Compound 1-2 (20mmol), Pd(dba) 2 (0.5mmol), tri-tert-butylphosphine (1.5mmol), and sodium tert-butoxide (40mmol) were dissolved in 200mL of anhydrous toluene, and stirred at 90°C for 3 hours under a nitrogen atmosphere. After the reaction was completed, 300 mL of water was added, separated, the aqueous phase was extracted with toluene, the organic phase was collected and dried with anhydrous magnesium sulfate, filtered, the solvent was spin-dried, and purified by column chromatography to obtain intermediate 1-3 with a yield of 75%.
[0108] Synthesis of Compound 1: Compound 1-3 (15mmol), Compound 1-4 (15mmol), Pd (dba) 2 (0.5mmol), tri-tert-butylphosphine (1.5mmol), and sodium tert-butoxide (30mmol) were dissolved in 180mL of anhydrous toluene, and stirred at 100°C for 6 hours under a nitrogen atmosphere. After the reaction was completed, 300 mL of water...
Embodiment 2
[0110] The synthesis of embodiment 2 compound 2
[0111]
[0112] The synthesis of compound 2 refers to the synthesis of compound 1, except that compound 1-4 is replaced by 2-1. MS (ASAP): 818.
Embodiment 3
[0113] The synthesis of embodiment 3 compound 3
[0114]
[0115] The synthesis of compound 3 was referred to the synthesis of compound 1, except that compound 1-4 was replaced by 3-1, and the yield was 81%.
[0116] Compound 3 was tested by mass spectrometry, MS (ASAP): 803, and the mass spectrogram is attached figure 2 shown.
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