Detection method of methyl bromoacetate
A kind of technology of methyl bromoacetate and detection method, applied in the detection field of methyl bromoacetate, can solve problems such as inability to learn from detection, and achieve the effect of being difficult to separate
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Embodiment 1
[0047] (1) The preparation method of the reference substance solution is to measure 1ml of methanol stock solution, 1ml of methyl methoxyacetate stock solution, 1ml of methoxyacetic acid stock solution, 1ml of bromoacetic acid stock solution and 1ml of methyl bromoacetate stock solution, and use Dilute with acetonitrile to 10ml, shake well, and obtain.
[0048] The preparation method of methanol stock solution is to take 50mg of methanol, dilute to 10ml with acetonitrile, shake well, and obtain;
[0049] The preparation method of methyl methoxyacetate stock solution is to take 50 mg of methyl methoxyacetate, dilute to 10 ml with acetonitrile, shake well, and obtain;
[0050] The preparation method of methoxyacetic acid stock solution is to take 50mg of methoxyacetic acid, dilute to 10ml with acetonitrile, shake well, and obtain;
[0051] The preparation method of bromoacetic acid stock solution is to take 50 mg of bromoacetic acid, dilute to 10 ml with acetonitrile, shake wel...
Embodiment 2
[0096] (1) The preparation method of the reference substance solution is to measure 1ml of methanol stock solution, 1ml of methyl methoxyacetate stock solution, 1ml of methoxyacetic acid stock solution, 1ml of bromoacetic acid stock solution and 1ml of methyl bromoacetate stock solution, and use Dilute with acetonitrile to 10ml, shake well, and obtain.
[0097] The preparation method of methanol stock solution is to take 50mg of methanol, dilute to 10ml with acetonitrile, shake well, and obtain;
[0098] The preparation method of methyl methoxyacetate stock solution is to take 50 mg of methyl methoxyacetate, dilute to 10 ml with acetonitrile, shake well, and obtain;
[0099] The preparation method of methoxyacetic acid stock solution is to take 50mg of methoxyacetic acid, dilute to 10ml with acetonitrile, shake well, and obtain;
[0100] The preparation method of bromoacetic acid stock solution is to take 50 mg of bromoacetic acid, dilute to 10 ml with acetonitrile, shake wel...
Embodiment 3
[0113] (1) The preparation method of the reference substance solution is to measure 1ml of methanol stock solution, 1ml of methyl methoxyacetate stock solution, 1ml of methoxyacetic acid stock solution, 1ml of bromoacetic acid stock solution and 1ml of methyl bromoacetate stock solution, and use Dilute with acetonitrile to 10ml, shake well, and obtain.
[0114] The preparation method of methanol stock solution is to take 50mg of methanol, dilute to 10ml with acetonitrile, shake well, and obtain;
[0115] The preparation method of methyl methoxyacetate stock solution is to take 50 mg of methyl methoxyacetate, dilute to 10 ml with acetonitrile, shake well, and obtain;
[0116] The preparation method of methoxyacetic acid stock solution is to take 50mg of methoxyacetic acid, dilute to 10ml with acetonitrile, shake well, and obtain;
[0117] The preparation method of bromoacetic acid stock solution is to take 50 mg of bromoacetic acid, dilute to 10 ml with acetonitrile, shake wel...
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