Silica gel, preparation method and protective film using silica gel
A technology of silicone gel and silicone oil, applied in the direction of adhesives, film/sheet adhesives, adhesive additives, etc., can solve the problems of no experimental data support, complex structure, unsatisfactory optical properties, etc., to achieve convenient production and use , The effect of the synthesis operation process is simple and the cost is low
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Embodiment 1
[0031] The silicone gel provided in this example, its raw materials include 100 parts by weight of vinyl polysiloxane, 20 parts of methyl MQ silicone resin, 0.8 parts of crosslinking agent, 0.6 parts of catalyst, 0.1 part of inhibitor, coupling 0.6 parts of agent and 150 parts of diluting solvent.
[0032] The vinyl polysiloxane used is terminal vinyl polysiloxane, and the specific chemical structure formula is ViMe 2 SiO(SiMe 2 O) n (SiMeViO) m SiMe 2 Vi, the vinyl content is 0.05wt%; Cross-linking agent adopts terminal hydrogen-containing silicone oil: hydrogen-terminated polydimethylmethylhydrogensiloxane, chemical structural formula is (CH 3 ) 2 (H)SiO[(CH 3 )(H)SiO] y Si(H)(CH 3 ) 2 , the hydrogen content is 0.17wt%, and the molar ratio of H in the silicon hydrogen group-containing silicone oil to the vinyl group is 0.8.
Embodiment 2
[0034] The silicone gel provided in this example, its raw materials include 100 parts by weight of vinyl polysiloxane, 20 parts of methyl MQ silicone resin, 1.1 parts of crosslinking agent, 0.6 parts of catalyst, 0.1 part of inhibitor, coupling 0.6 parts of agent and 150 parts of diluting solvent.
[0035] The vinyl polysiloxane used is terminal vinyl polysiloxane, and the specific chemical structure formula is ViMe 2 SiO(SiMe 2 O) n (SiMeViO) m SiMe 2 Vi, the vinyl content is 0.05wt%; Cross-linking agent adopts terminal hydrogen-containing silicone oil: hydrogen-terminated polydimethylmethylhydrogensiloxane, chemical structural formula is (CH 3 ) 2 (H)SiO[(CH 3 )(H)SiO] ySi(H)(CH 3 ) 2 , the hydrogen content is 0.17wt%, and the molar ratio of H in the silicone oil containing silicon hydrogen group to the vinyl group is 1.0.
Embodiment 3
[0037] The silica gel provided in this embodiment, its raw materials include 100 parts by weight of vinyl polysiloxane, 20 parts of methyl MQ silicone resin, 1.4 parts of crosslinking agent, 0.6 parts of catalyst, 0.1 part of inhibitor, coupling 0.6 parts of agent and 40 parts of diluting solvent.
[0038] The vinyl polysiloxane used is terminal vinyl polysiloxane, and the specific chemical structure formula is ViMe 2 SiO(SiMe 2 O) n (SiMeViO) m SiMe 2 Vi, the vinyl content is 0.05wt%; Cross-linking agent adopts terminal hydrogen-containing silicone oil: hydrogen-terminated polydimethylmethylhydrogensiloxane, chemical structural formula is (CH 3 ) 2 (H)SiO[(CH 3 )(H)SiO] y Si(H)(CH 3 ) 2 , the hydrogen content is 0.17wt%, and the molar ratio of H in the silicone oil containing silicon hydrogen group to the vinyl group is 1.3.
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