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Vitrification agent, preparation method thereof and vitrification process

A vitrifying agent and process technology, which is applied in the direction of metal material coating process, etc., can solve the problems of poor adhesion, short salt spray resistance time, poor corrosion resistance, etc., to prolong the corrosion resistance time, excellent rust resistance, Avoid the effect of returning rust

Pending Publication Date: 2022-06-03
万春雷
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The composition of the vitrifying agent is particularly important to the vitrification effect of the workpiece. The existing vitrified workpieces are prone to rust, poor corrosion resistance, short salt spray resistance time, poor adhesion, etc. In view of this, it is necessary to modify the existing technology A kind of vitrifying agent is improved to solve the above-mentioned technical problems

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] The present embodiment discloses a ceramizer and its preparation method and ceramization process, which specifically include the following contents:

[0032] The ceramic agent comprises the following components in parts by weight: 5 parts of fluorozirconic acid, 15 parts of bisaminosilane, 6 parts of monoethanolamine borate, 1 part of sodium nitrite, 3 parts of pH adjuster, and 50 parts of water . The water is deionized water, and the pH adjusting agent is ammonia water.

[0033] The preparation method of the potting agent comprises the following steps:

[0034] Step 1: Weigh each component according to parts by weight;

[0035] Step 2: Add 70% water into the mixing tank, then add fluorozirconic acid, bisaminosilane, monoethanolamine borate, and sodium nitrite in sequence, stir evenly to obtain a pre-mixed solution, and the stirring time is 0.5h;

[0036] Step 3: Add the remaining 30% of water to the tank;

[0037] Step 4: detecting the pH value of the pre-preparati...

Embodiment 2

[0047] The present embodiment discloses a ceramizer and its preparation method and ceramization process, which specifically include the following contents:

[0048] The ceramic agent comprises the following components in parts by weight: 8 parts of fluorozirconic acid, 20 parts of bisaminosilane, 10 parts of monoethanolamine borate, 4 parts of sodium nitrite, 9 parts of pH adjuster, and 80 parts of water . The water is tap water, and the pH adjuster is sodium hydroxide.

[0049] The preparation method of the potting agent comprises the following steps:

[0050] Step 1: Weigh each component according to parts by weight;

[0051] Step 2: Add 70% water into the mixing tank, then add fluorozirconic acid, bisaminosilane, monoethanolamine borate, and sodium nitrite in sequence, and stir evenly to obtain a pre-mixed solution, and the stirring time is 1 h;

[0052] Step 3: Add the remaining 30% of water to the tank;

[0053] Step 4: Detecting the pH value of the pre-preparation so...

Embodiment 3

[0063] The present embodiment discloses a ceramizer and its preparation method and ceramization process, which specifically include the following contents:

[0064] The ceramic agent comprises the following components in parts by weight: 10 parts of fluorozirconic acid, 25 parts of bisaminosilane, 15 parts of monoethanolamine borate, 7 parts of sodium nitrite, 16 parts of pH adjuster, and 100 parts of water . The water is deionized water, and the pH adjusting agent is ammonia water.

[0065] The preparation method of the potting agent comprises the following steps:

[0066] Step 1: Weigh each component according to parts by weight;

[0067] Step 2: add 70% water into the mixing tank, then add fluorozirconic acid, bisaminosilane, monoethanolamine borate, and sodium nitrite in sequence, and stir evenly to obtain a pre-mixed solution, and the stirring time is 1.5h;

[0068] Step 3: Add the remaining 30% of water to the tank;

[0069] Step 4: Detecting the pH value of the pre-pr...

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Abstract

The invention provides a vitrification agent, a preparation method thereof and a vitrification process. The vitrification agent comprises the following components in parts by weight: 5-10 parts of hexafluorozirconic acid, 15-25 parts of diamino silane, 6-15 parts of monoethanolamine borate, 1-7 parts of sodium nitrite, 3-16 parts of a pH regulator and 50-100 parts of water. According to the vitrification agent and the preparation method thereof and the vitrification process, by introducing the monoethanolamine borate, a compact and uniform vitrification film layer with excellent anti-rust performance can be generated on the surface of a workpiece, the phenomena of re-rusting, dust sticking and the like after the workpiece is subjected to vitrification treatment are effectively avoided, and the requirements before coating are met; the salt spray test time of the ceramic workpiece can be more than 500 hours, excellent adhesive force can be provided for the combination of the workpiece and various coatings, the corrosion resistance time of the workpiece is prolonged, and the impact resistance is relatively strong.

Description

technical field [0001] The invention relates to the technical field of potting procedures, in particular to a potting agent, a preparation method thereof, and a potting process. Background technique [0002] Metal workpieces usually need to be pre-treated including degreasing, rust removal, etc. before coating. In addition, a chemical conversion film needs to be formed on the surface of the metal workpiece during the pre-treatment. The conversion film has a certain anti-corrosion ability and can avoid parts. Rusting back in a short time before spraying can also increase the roughness of the surface of the part and enhance the bonding force between the coating and the substrate. The existing processes for this treatment are mainly phosphating process, pottery process, surface silanization process and organic film pretreatment process. [0003] Among them, in the existing pottery process, the metal workpiece is immersed in a potting solution containing fluorozirconic acid or ...

Claims

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Application Information

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IPC IPC(8): C23C22/34C23C22/73C23C22/76C23C22/78
CPCC23C22/34C23C22/73C23C22/76C23C22/78Y02E60/50
Inventor 万春雷
Owner 万春雷
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