Polymer microsphere with high refractive index and preparation method thereof
A high refractive index, polymer technology, applied in the field of biomedicine, can solve the problems of inconvenient preparation, poor refractive index properties of latex microspheres, etc., and achieve the effects of low production cost, excellent hand feel and elongation, and improved mechanical properties.
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Embodiment 1
[0029] Embodiment 1, a high-refractive-index polymer microsphere, including the following raw materials in parts by weight: 100 parts of aliphatic conjugated diene monomers, 10 parts of ethylenically unsaturated carboxylic acid monomers, and 100 parts of acrylonitrile monomers. 20 parts of body, 10 parts of medium chain fatty acid glycerides and 5-15 parts of aluminum compound aqueous solution.
Embodiment 2
[0030] Embodiment 2, a high-refractive-index polymer microsphere, comprising the following raw materials in parts by weight: 150 parts of aliphatic conjugated diene monomers, 50 parts of ethylenically unsaturated carboxylic acid monomers, acrylonitrile monomers 30 parts of body, 20 parts of medium chain fatty acid glycerides and 10 parts of aluminum compound aqueous solution.
Embodiment 3
[0031] Embodiment 3, a high-refractive-index polymer microsphere, comprising the following raw materials in parts by weight: 200 parts of aliphatic conjugated diene monomers, 100 parts of ethylenically unsaturated carboxylic acid monomers, and acrylonitrile monomers. 40 parts of body, 30 parts of medium chain fatty acid glycerides and 15 parts of aluminum compound aqueous solution.
[0032] A preparation method of high refractive index polymer microspheres, comprising the following steps:
[0033] 1) Preparation of solution: water phase solution: send the metered emulsifier and water to the water phase solution preparation tank respectively, and the water phase solution prepared after stirring and fully mixing; oil phase solution: place styrene in an organic solvent Dissolve in the solution, feed nitrogen into the solution to remove oxygen to obtain an oil phase solution;
[0034] 2) Preparation of latex: put an appropriate amount of initiator, aliphatic conjugated diene mono...
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