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Method for detecting Kidney tonifying mind easing extractive quality standard

A technology of quality standards and detection methods, applied in the field of medicine, can solve problems such as inability to effectively guarantee the inherent quality of products and the lack of guarantee of drug efficacy.

Inactive Publication Date: 2007-06-06
SHANGHAI LEIYUNSHANG PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In the original quality standard, the eight herbs such as ginseng were qualitatively identified, but there were no content measurement items for the index components that reflected the internal quality of the drug, and the internal quality of the product could not be effectively guaranteed during production, and the efficacy of the drug could not be guaranteed.

Method used

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  • Method for detecting Kidney tonifying mind easing extractive quality standard
  • Method for detecting Kidney tonifying mind easing extractive quality standard
  • Method for detecting Kidney tonifying mind easing extractive quality standard

Examples

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Effect test

example 1

[0065] Example 1, batch number 030901

[0066] 1. TLC identification of loquat leaves

[0067] Take 100g of this product, put it in a conical flask, add 200ml of solvent (methanol, ethanol, water, n-butanol or chloroform), shake well, extract (ultrasonic treatment or heat reflux or cold soaking) for 20 minutes, let cool, filter After drying, the filtrate was evaporated to dryness, and the residue was dissolved by adding 80ml of water, extracted twice by shaking with n-butanol saturated with water, 50ml each time, combined with the n-butanol liquid, washed twice with n-butanol-saturated water, 80ml each time, discarded Remove water, recover n-butanol to dryness, add 1ml of solvent (methanol, ethanol, water, n-butanol or chloroform) to dissolve the residue, and use it as the test solution. Take another 2 g of loquat leaf reference medicinal material, add solvent (methanol, ethanol, water, n-butanol or chloroform) 30 ml, extract (ultrasonic treatment or heat reflux or cold immer...

example 2

[0078] Batch number: 030902

[0079] According to the 030901 batch test, the test results: (1) positive for identification, (2) Danshen (based on protocatechualdehyde (C 7 h 6 o 3 ) in total) 19.84 μg.

example 3

[0081] Batch number: 031001

[0082] According to the 030901 batch test, the test results: (1) positive for identification, (2) Danshen (based on protocatechualdehyde (C 7 h 6 o 3 ) in total) 21.35 μg.

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Abstract

This invention relates to Chinese medicine filed, which discloses one medicine easy for kidney and mentality quality testing method. The invention improves the original quality standard and adds loquat identification by nature and establishes radix salvia miltiorrhiza protocatechualdehyde content testing.

Description

Technical field: [0001] The invention belongs to the technical field of medicine. It specifically relates to the quality standard detection method of Yishen Anshen Ointment. Background technique: [0002] Yishen Anshen Ointment is a traditional decoction, which is composed of ginseng, pearl powder, Nansha ginseng, Beisha ginseng, salvia miltiorrhiza, astragalus, Schisandra (made), mulberry, Ligustrum lucidum (made), angelica, epimedium, Cyperus cyperi ( Composition of twenty-six traditional Chinese medicines such as Ganoderma lucidum, Gansong, Millet, Mussel, Iris, Polygala (made), oyster, Dipsacus, Polygonum cuspidatum, loquat leaf, tangerine peel, rehmannia glutinosa, malt, rice bud, etc. It has the effects of nourishing qi and blood, nourishing the kidney and calming the nerves. It is used for dizziness, weakness of the waist and knees, night sweat and insomnia caused by deficiency of Qi and blood; it can also be used for postpartum and post-ill care. In the prescripti...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/28G01N30/06G01N30/94G01N1/28
Inventor 徐福莺邵宝平谢松沈绣红
Owner SHANGHAI LEIYUNSHANG PHARMA