Extraction method of Anhui fritillary extract
An extraction method and extraction technology, applied in the extraction field of Fritillaria fritillata extract, can solve the problems of different content, influence on curative effect, large dose, etc.
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[0021] Below with the hydrochloric acid of 0.2mol / L concentration as example, limited embodiment is described as follows:
[0022] 1. Percolation
[0023] Take dried fritillary bulbs, coarsely crush them to obtain coarse powder, or slice them to obtain flakes, place them in a percolator, percolate with hydrochloric acid, and collect percolation liquid. The amount of hydrochloric acid is about 10 to 15 times the amount of medicinal materials.
[0024] When using different concentrations of hydrochloric acid or other protic acids, the settings and procedures used are the same.
[0025] 2. Separation
[0026] (1) Neutralize the percolation liquid with dilute alkali to pH 7.2-7.5, then extract it with ethanol for 4-5 times in the extractor, and combine the extracts to obtain the ethanol solution of the extract.
[0027] (2) The X-5 macroporous adsorption resin is used for pretreatment and then loaded into the column. The pretreatment is to wash with medical ethanol, and then to...
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