Fine carbon fiber mixture and composition thereof
A technology of carbon fibers and mixtures, applied in fiber processing, fiber chemical characteristics, textiles and papermaking, etc., can solve problems that are not suitable for large-scale production
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[0069] The present invention will be described below by way of examples.
[0070] (Example)
[0071] Such as figure 1 As shown schematically, the raw material feed pipe 4 and the carrier gas feed pipe 6 for adding the raw material gasified in the raw material gasification device 5 are arranged on the top of the vertical heating furnace 1 (inner diameter: 170mm, length: 1500mm) .
[0072]Benzene containing ferrocene (4% by mass) and thiophene (5% by mass (1.9% by mass when converted to atomic sulfur)) was gasified, and the gasified product was fed through the raw material feed pipe 4 at a rate of 15 g / min. , while maintaining the temperature of the product at 200°C, and hydrogen gas serving as a carrier gas was fed at a rate of 180 liters / minute, thereby allowing the reaction to proceed.
[0073] The fine carbon fibers produced by the above reaction were heat-treated at 1300° C. in an argon (Ar) atmosphere. The thus-treated fine carbon fibers were further subjected to heat ...
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