Modified active carbon fiber used as filtering material to lower toxic matter from cigartte, and its prepn. method
A technology of activated carbon fibers and cigarettes, which is applied in e-liquid filter elements, applications, tobacco, etc., can solve the problems of poor filtration effect, no CO purification, and inability to proportionally reduce tar and nicotine, so as to reduce harmfulness, smoke alcohol and nicotine. Effect
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[0012] Example 1: Add ethylene glycol monomethyl ether to a titanium sulfate solution with a titanium sulfate mass fraction of 2%. The amount of ethylene glycol monomethyl ether added is 0.3% of the weight of the titanium sulfate solution. After stirring, add the viscose base Activated carbon fiber (ACF), the amount of ACF added is 2% of the mass of the titanium sulfate solution, heated to 85°C, and after another 1 hour, add saturated ammonia bicarbonate solution, adjust the pH value of the feed solution to 5-6, and use deionization Rinse with water to pH 6.5~7.5, take out the ACF and put it into an oven to bake at 120℃ for 1 hour, and place it in a muffle furnace under the protection of nitrogen (normal pressure) and sinter at 400℃ for 1 hour , And then cooled to room temperature below 40°C. Put the obtained ACF into PdCl 2 And CuCl mixed aqueous solution, the PdCl in the mixed aqueous solution 2 The mass fractions of CuCl and CuCl are 0.02% and 0.2%, respectively, and the rest i...
Example Embodiment
[0013] Example 2: Add ethylene glycol monomethyl ether to a titanium sulfate solution with a titanium sulfate mass fraction of 2%. The amount of ethylene glycol monomethyl ether added is 0.4% of the weight of the titanium sulfate solution. After stirring evenly, add activated carbon fiber ( ACF), the amount of ACF added is 2.5% of the mass of the titanium sulfate solution, heat to 90°C, add saturated ammonia bicarbonate solution after another 1.5 hours, adjust the pH value of the feed solution to 5-6, and rinse with deionized water to pH to 6.5~7.5, take out the ACF and put it in the oven at 130℃ for 1.5 hours, put it in a muffle furnace under nitrogen (normal pressure) protection, sinter at 450℃ for 1.5 hours, then cool To room temperature below 40℃. Put the obtained ACF into PdCl 2 And CuCl mixed aqueous solution, the PdCl in the mixed aqueous solution 2 The mass fractions of CuCl and CuCl are 0.04% and 0.2%, respectively, and the rest is water. The amount of ACF added is PdCl 2...
Example Embodiment
[0014] Example 3: Add ethylene glycol monomethyl ether to a titanium sulfate solution with a titanium sulfate mass fraction of 3%. The addition amount of ethylene glycol monomethyl ether is 0.5% of the weight of the titanium sulfate solution. After stirring, add activated carbon fiber ( ACF), the amount of ACF added is 3% of the mass of the titanium sulfate solution, heat to 95°C, add saturated ammonia bicarbonate solution after another 1.5 hours, adjust the pH value of the feed solution to 5-6, and rinse with deionized water to pH to 6.5~7.5, take out the ACF and put it into the oven to bake at 150℃ for 2 hours, put it in the muffle furnace under the protection of nitrogen (normal pressure) and sinter at 500℃ for 1.5 hours, then cool down To room temperature below 40°C. Put the obtained ACF into PdCl 2 And CuCl mixed aqueous solution, the PdCl in the mixed aqueous solution 2 The mass fractions of CuCl and CuCl are respectively 0.05% and 0.4%, and the rest is water. The amount of ...
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