Modified active carbon fiber used as filtering material to lower toxic matter from cigartte, and its prepn. method

A technology of activated carbon fibers and cigarettes, which is applied in e-liquid filter elements, applications, tobacco, etc., can solve the problems of poor filtration effect, no CO purification, and inability to proportionally reduce tar and nicotine, so as to reduce harmfulness, smoke alcohol and nicotine. Effect

Inactive Publication Date: 2005-11-09
NANJING NORMAL UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The United States and Japan have developed activated carbon fiber or composite activated carbon fiber cigarette filters. Although they have obvious filtering effects on tar, nicotine, fatty aldehydes, etc., they have poor filtering effects on strong carcinogens such as benzo[a]pyrene. , has almost no purification effect on

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0012] Example 1: Add ethylene glycol monomethyl ether to a titanium sulfate solution with a titanium sulfate mass fraction of 2%. The amount of ethylene glycol monomethyl ether added is 0.3% of the weight of the titanium sulfate solution. After stirring, add the viscose base Activated carbon fiber (ACF), the amount of ACF added is 2% of the mass of the titanium sulfate solution, heated to 85°C, and after another 1 hour, add saturated ammonia bicarbonate solution, adjust the pH value of the feed solution to 5-6, and use deionization Rinse with water to pH 6.5~7.5, take out the ACF and put it into an oven to bake at 120℃ for 1 hour, and place it in a muffle furnace under the protection of nitrogen (normal pressure) and sinter at 400℃ for 1 hour , And then cooled to room temperature below 40°C. Put the obtained ACF into PdCl 2 And CuCl mixed aqueous solution, the PdCl in the mixed aqueous solution 2 The mass fractions of CuCl and CuCl are 0.02% and 0.2%, respectively, and the rest i...

Example Embodiment

[0013] Example 2: Add ethylene glycol monomethyl ether to a titanium sulfate solution with a titanium sulfate mass fraction of 2%. The amount of ethylene glycol monomethyl ether added is 0.4% of the weight of the titanium sulfate solution. After stirring evenly, add activated carbon fiber ( ACF), the amount of ACF added is 2.5% of the mass of the titanium sulfate solution, heat to 90°C, add saturated ammonia bicarbonate solution after another 1.5 hours, adjust the pH value of the feed solution to 5-6, and rinse with deionized water to pH to 6.5~7.5, take out the ACF and put it in the oven at 130℃ for 1.5 hours, put it in a muffle furnace under nitrogen (normal pressure) protection, sinter at 450℃ for 1.5 hours, then cool To room temperature below 40℃. Put the obtained ACF into PdCl 2 And CuCl mixed aqueous solution, the PdCl in the mixed aqueous solution 2 The mass fractions of CuCl and CuCl are 0.04% and 0.2%, respectively, and the rest is water. The amount of ACF added is PdCl 2...

Example Embodiment

[0014] Example 3: Add ethylene glycol monomethyl ether to a titanium sulfate solution with a titanium sulfate mass fraction of 3%. The addition amount of ethylene glycol monomethyl ether is 0.5% of the weight of the titanium sulfate solution. After stirring, add activated carbon fiber ( ACF), the amount of ACF added is 3% of the mass of the titanium sulfate solution, heat to 95°C, add saturated ammonia bicarbonate solution after another 1.5 hours, adjust the pH value of the feed solution to 5-6, and rinse with deionized water to pH to 6.5~7.5, take out the ACF and put it into the oven to bake at 150℃ for 2 hours, put it in the muffle furnace under the protection of nitrogen (normal pressure) and sinter at 500℃ for 1.5 hours, then cool down To room temperature below 40°C. Put the obtained ACF into PdCl 2 And CuCl mixed aqueous solution, the PdCl in the mixed aqueous solution 2 The mass fractions of CuCl and CuCl are respectively 0.05% and 0.4%, and the rest is water. The amount of ...

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PUM

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Abstract

A modified activated carbon fiber (ACF), TiO2-Pd-Cu based ACF, for filtering out the tar, nicotin, CO, benzo(a) pyrene, fatty aldehyde, etc from the smoke of cigarette is prepared through adding ethanediol monomether into the solution of titanium sulfate, stirring, adding ACF, heating, adding the saturated solution of ammonium dicarbonate, regulating pH value, baking ACF, sintering, cooling, immersing in the aqueous solution of PbCl2 and CuCl, baking and cooling.

Description

technical field [0001] The invention relates to a filter material for a cigarette filter tip and a preparation method thereof, in particular to a modified active carbon fiber used for cigarette filter harm reduction and a preparation method thereof. Background technique [0002] Cigarette smoke contains harmful substances such as tar and CO. At present, the contents of the above two components in most domestic flue-cured cigarettes are: 15-17mg / stick, 14-16mg / stick. On May 21, 2003, the "Framework Convention on Tobacco Control" was adopted at the 56th World Health Assembly. On November 10, 2003, the Chinese government signed the "Framework Convention on Tobacco Control". The Chinese government promised that cigarettes produced after July 1, 2004, with a tar content of more than 15 mg per stick will not enter the sales market; The average tar content of cigarettes is reduced to about 12 mg / stick. However, the tar not only contains some harmful substance...

Claims

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Application Information

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IPC IPC(8): A24D3/10
Inventor 张玉清庄磊顾中铸
Owner NANJING NORMAL UNIVERSITY
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