Method of manufacturing for electrolyte membrane electrode joint body for fuel cell
An electrolyte membrane electrode and fuel cell technology, which is applied to fuel cell parts, battery electrodes, solid electrolyte fuel cells, etc., can solve problems such as catalyst layer cracking, fuel cell failure to obtain satisfactory battery characteristics, and mutual contamination of catalyst layers.
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Embodiment 1
[0095] 1(a)-(e), an intermediate body 9 of an electrolyte membrane-electrode assembly having catalyst layers 4a and 4b formed on both sides of a proton-conducting polymer membrane 1 is produced, and a fuel cell is manufactured using it. First, a proton-conducting polymer membrane 1 with a film thickness of 30 μm is laminated on a first shape-retaining film 2 composed of a polyethylene terephthalate film with a film thickness of 190 μm to form a shape-retaining film as shown in FIG. 1( a ). Intermediate 3. The proton conductive polymer membrane 1 is made of perfluorocarbon sulfonic acid represented by the following formula (where x=5 to 13.5, y≈1000, m=1, n=2).
[0096]
[0097]The above proton conductive polymer membrane 1 is laminated on the first shape retaining membrane 2 by a so-called transfer method. Specifically, first, the proton-conducting polymer membrane 1 and the first shape-retaining membrane 2 formed in advance on a support membrane by a casting process are s...
Embodiment 2
[0108] 1(a)-(e), an intermediate body 9 of an electrolyte membrane-electrode assembly having catalyst layers 4a and 4b formed on both sides of a proton-conducting polymer membrane 1 is produced, and a fuel cell is manufactured using it.
[0109] First, an ethanol dispersion containing 91% by weight of the same perfluorocarbon sulfonic acid as used in Example 1 was coated on the first shape-retaining film 2 made of a polypropylene film with a film thickness of 50 μm, and dried. The speed of conveying the first shape-retaining film was set at 0.7 m / min. Coating method is blade height 0.16mm, overcoat 3 times. The coating film was left to dry at room temperature to form a proton-conducting polymer film 1 with a film thickness of 30 μm on the first shape-retaining film 2 . The intermediate 3 shown in Fig. 1(a) was produced by the above method.
[0110] There was almost no warpage or deformation in the intermediate body 3, and no damage such as microcracks or pinholes was observe...
Embodiment 3
[0117] according to image 3 In the order of (a) to (e), the catalyst layers 4a and 4b are respectively formed on both sides of the proton conductive polymer membrane 1, and the intermediate body 24 of the electrolyte membrane electrode assembly formed by combining the catalyst layers 4a and 4b with the gaskets 20a and 20b, and further Use it to make fuel cells.
[0118] First of all, it is made by the same method as in Example 1 image 3 (a) Intermediate 3 shown. In the intermediate body 3, there was almost no warpage or deformation, and no damage such as microcracks or pinholes was observed even in the proton conductive polymer membrane 1 itself, and the condition was good. In this intermediate body 3, the proton-conducting polymer membrane 1 and the holding membrane 2 are properly adhered to each other, so they cannot be peeled off even if they are bent with a radius of curvature (R) of about 50 mm. Then, make it with exactly the same method as Example 1 image 3 Interm...
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Abstract
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