Production process of high purity aluminium foil for electrolytic capacity
An electrolytic capacitor and production process technology, applied in electrolytic capacitors, capacitors, circuits, etc., can solve the problems of poor quality and poor performance of electronic aluminum foil, achieve good economic and social benefits, curb price rises, and be very internationally competitive. Effect
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Embodiment 1
[0021] Get 200mm (length) * 50mm (width) * 7.5mm (thick) high-purity aluminum (Al≥99.99%Wt.) hot-rolled plate, press 1.06 speed ratio, present embodiment adopts 4 pass rolling, rolling The pressing amount is 40%, 30%, 20%, and 9.2% in turn, and the deformation amount reaches 99.2% and is asynchronously cold-rolled into high-purity aluminum foil. Wash with NaOH solution, mark the rolling direction, and obtain the cold-rolled texture sample. Put the cold-rolled sample into the pass with N 2 In the tubular annealing furnace with protective gas, the temperature was raised with the furnace at a heating rate of 10°C / min. When the temperature rises to 600°C, it is kept for 3 hours and quenched in water to obtain an annealed texture sample.
[0022] The texture of the cold-rolled and annealed samples was measured respectively. The texture was measured on the D / max-IIIA X-ray diffractometer and the B-7 semi-automatic texture measuring angle table in the Northeastern University Test C...
Embodiment 2
[0024] Get 200mm (length) * 50mm (width) * 7.5mm (thick) high-purity aluminum hot-rolled plate, according to the speed ratio of 1.17, the present embodiment adopts 3 pass rolling, and the amount of rolling down is 45% successively , 35%, 18.7%, reaching a deformation of 98.7% asynchronously cold-rolled into high-purity aluminum foil, the size after rolling is 0.1mm thick, cut a 20mm×20mm sample, clean the surface with NaOH solution, mark the rolling direction, and obtain a cold As-rolled texture samples. Put the cold-rolled sample into the pass with N 2 In the tubular annealing furnace with protective gas, the temperature was raised with the furnace at a heating rate of 10°C / min. When the temperature rose to 500°C, it was kept for 2 hours and quenched in water to obtain an annealed texture sample. The cubic texture volume fraction of the high-purity aluminum foil prepared by the process is measured to be 95.0%.
Embodiment 3
[0026] Get 200mm (length) * 50mm (width) * 7.5mm (thick) high-purity aluminum hot-rolled plate, according to the speed ratio of 1.17, the present embodiment adopts 3 pass rolling, and the rolling down force is 42% successively , 38%, and 16.7%, reaching 96.7% of deformation, asynchronously cold-rolled into high-purity aluminum foil. As-rolled texture samples. Put the cold-rolled sample into the pass with N 2 In the tubular annealing furnace with protective gas, the temperature is raised with the furnace at a heating rate of 5°C / min. When the temperature rises to 400°C, it is kept for 2 hours and quenched in water to obtain an annealed texture sample. The cubic texture volume fraction of the high-purity aluminum foil prepared by the process is measured to be 95.57%.
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