Sintered body, magnetic head slider, and method of manufacturing sintered body
A manufacturing method and technology of sintered body, applied in the direction of nanotechnology, nanotechnology, nanotechnology, etc. for material and surface science, to achieve the effect of sufficient grinding speed and reducing step difference
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Embodiment 1~3
[0102] Weigh alumina powder (average particle size 320nm) and carbon powder (carbon black, average primary particle size 15nm) according to the specified amount respectively, pulverize together with IPA (isopropanol; boiling point 82.4°C) in a ball mill for 30 minutes and carry out After mixing, spray granulation was performed at 150° C. in nitrogen to obtain a granulated product.
[0103] Here, alumina powder and carbon powder were mixed in the granulated material at a concentration satisfying the following conditions. That is, when the weight of the alumina powder is 100 parts by weight, the weight of the carbon powder is 0.5 parts by weight in Example 1, 1.5 parts by weight in Example 2, and 3.1 parts by weight in Example 3.
[0104] Next, the obtained granules were heated at about 0.5MPa (50kgf / cm 2 ) under the pressure of a forming. Then, use the hot pressing method in a vacuum atmosphere and a spray pressure of about 30MPa (about 300kgf / cm 2 ) under sintering for 1 ho...
Embodiment 4~6
[0108] In Examples 4 to 6, except that carbon black having an average primary particle diameter of 100 nm was used as the carbon powder, the others were the same as in Comparative Examples 1 to 3.
Embodiment 7~9
[0112]In Examples 7 to 9, except that alumina powder, carbon powder, and titanium carbide powder (average primary particle size: 300 nm) were mixed, and the sintering temperature and mixing ratio were set as follows, the others were the same as in Example 1. In Example 7, when the weight of alumina powder is 100 parts by weight, the weight of carbon powder is 0.8 parts by weight, the weight of titanium carbide powder is 56.3 parts by weight, and the sintering temperature is 1700°C. In Example 8, the weight of carbon powder is 2.3 parts by weight, the weight of titanium carbide powder is 56.3 parts by weight, and the sintering temperature is 1720°C. In Example 9, the weight of carbon powder is 4.0 parts by weight, the weight of titanium carbide powder is 56.2 parts by weight, and the sintering temperature is 1720°C. In addition, about 0.1% of carbon based on the weight of titanium carbide is unavoidably contained in the titanium carbide powder, but since the amount is small, it...
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