Identification and assaying method for extractive of flowers and leaves of pseudo-ginseng
An identification method and extract technology, applied in pharmaceutical applications, preparation of Radix Ginseng flower leaf extract, protopanaxadiol ginsenoside field, can solve the unstable content of active ingredients in the extract and the lack of quality control indicators , patients taking inconvenience and other problems, to achieve perfect quality standards, improve process and quality standards, stable product quality and excellent results
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Embodiment 1
[0209] Extract the pulverized Tianqi flower leaves twice at 80°C with water heat, concentrate under reduced pressure to obtain an extract with a relative density of 1.07. Mix the extract with 2 times the weight of macroporous adsorption resin JKSD and put it on the column. 5 times column volume of clean water was eluted until colorless, and discarded this part of the eluate. Continue washing with 95% ethanol until colorless, collected the eluate, and obtained the total saponins of Radix chinensis. After measuring the content of ginsenoside Rb1, determine the content of excipients. Add appropriate amount of starch and corresponding excipients to the total saponins of Panax chinensis leaves, mix well, granulate, and press into tablets. The daily dosage of ginsenoside Rb1 is not less than 8mg. It has the effects of clearing away heat, cooling blood, calming the liver, and suppressing yang. It has a good therapeutic effect on acne vulgaris, especially acne vulgaris with blood heat ...
Embodiment 2
[0211] Extract with 60% ethanol solution, heat reflux at 60-70°C for 2 hours, and keep stirring. Extract 3 times. The extract was concentrated under reduced pressure to a relative density of 1.06 (45°C-50°C) extract to obtain a crude extract. The crude extract and the macroporous adsorption resin Amberlite XAD16 in equal weight were mixed well and put on the column, and 5 times column volume of clean water was eluted until colorless, and this part of the eluate was discarded. Continue to rinse with 90% ethanol until it becomes colorless, collect the eluate, and dry it under reduced pressure to obtain the total saponins from the leaves of Seven Flowers. The total saponins of Panax chinensis leaves can be measured for the content of ginsenoside Rb3 to determine the content of auxiliary materials, starch and corresponding auxiliary materials are added, mixed and put into capsules to make capsules. The daily dosage of ginsenoside Rb3 is not less than 16mg. It has the effects of...
Embodiment 3
[0213] Extract Tianqi flower leaves with hot water at 100°C under reflux for 2 to 4 hours, a total of three times. The extract is concentrated under reduced pressure to a relative density of 1.08 (45-50°C) extract. The crude extract and the equal weight of macroporous adsorption resin DA101 were mixed well and put on the column, and 5 times column volume of clean water was eluted until colorless, and this part of the eluate was discarded. Continue to wash with 95% ethanol until it becomes colorless, collect the eluate, and obtain the total saponins from the leaves of Seven Flowers. Vacuum dry. After grinding, determine the content of excipients according to the total content of ginsenosides Rb1, Rb2 and Rb3, add micropowder silica gel and starch, mix and press into tablets to make tablets. The total daily dose of ginsenosides Rb1, Rb2, and Rb3 is not less than 24mg. It has the effects of clearing heat, cooling blood, calming the liver, and suppressing yang. It has a good t...
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