Resin compound of containing addition product of benzoquinone-cyclopentadiene, and composition of photoresistive agent of containing the resin compound
A technology of composition and compound, which is applied in the direction of optics, optomechanical equipment, photoplate process of patterned surface, etc., can solve problems such as insufficient mechanical strength, insufficient panel strength, gap inhomogeneity, panel color change, etc.
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[0058] the term:
[0059] LAH: lithium aluminum oxide ("lithium aluminum hydride")
[0060] BQDCPOH: 1, 4, 4a, 5, 8, 8a, 9, 9a, 10, 10a-decahydro-1, 4: 5, 8-dimethyl bridge-9, 10-diol ("1, 4, 4a , 5,8,8a,9,9a,10,10a-decahydro-1,4:5,8-dimethanoanthracene-9,10-diol")
[0061] Preparation of benzoquinone-cyclopentadiene adduct:
[0062] (1) Freshly prepared cyclopentadiene (26.4 g, 0.4 mol) was added to a solution of p-benzoanthracene (21.6 g, 0.2 mol) in ethanol (200 mol), and the mixture was stirred for half an hour. The resulting colorless solid was filtered and washed with cold ethanol to obtain almost completely reacted dicyclopentadiene-benzoquinone adduct (BQDCP).
[0063] (2) Take the aforementioned product (24 grams, 10 moles) and add LAH (4 grams, 100 moles) in ether (200 milliliters) solution, after reflux reaction for 8 hours, terminate the reaction with aqueous sodium hydroxide solution to obtain the diol product (BQDCPOH).
[0064] (3) Add 6 grams of sodium hyd...
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