A refined fur seal enriched in OMEGA-3 polyunsaturated fatty acid and preparation thereof
A technology of unsaturated fatty acids and seal oil, applied in the field of medicine, can solve the problems of weakened and incomplete drug effects, and achieve the effect of high concentration
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Embodiment 1
[0027] Refined seal oil: containing OMEGA3 polyunsaturated fatty acid DPA 8.31%, EPA 11.29%, DHA 18.12% (weight percentage), the sum of the three is 37.72%.
[0028] This refining seal oil is made by following method:
[0029] Equipment: German VTA short-range molecular distillation apparatus with a distillation area of 0.4m 2 .
[0030] Raw materials: crude seal oil, the sum of DPA, EPA, and DHA is 16.84%, provided by Tianjin Tasly Modern Chinese Medicine Resources Co., Ltd.
[0031] Operating conditions: two-stage vacuum distillation is adopted, the pressure of the first polar molecular still is 5Pa, the evaporation temperature is 140°C, and the speed of the wiped film rotor is 100rpm; the pressure of the second polar molecular still is 0.3Pa, and the evaporation temperature is 300°C. The speed of the wiped film rotor was 250 rpm; the feed rate was 7 kg / hour. The seal oil crude oil passes through the wiped film evaporator, the low boiling point components are evaporated...
Embodiment 2
[0033] Refined seal oil: containing OMEGA3 polyunsaturated fatty acid DPA 6.56%, EPA 8.21%, DHA 16.32% (percentage by weight), the sum of the three is 31.09%.
[0034] This refining seal oil is made by following method:
[0035] Equipment: same as embodiment one.
[0036] Raw material: with embodiment one.
[0037] Operating conditions: two-stage vacuum distillation is adopted, the pressure of the first polar molecular still is 10Pa, the evaporation temperature is 130°C, and the rotating speed of the wiped film rotor is 100rpm; the pressure of the second polar molecular still is 0.5Pa, and the evaporation temperature is 25°C. The speed of the wiped film rotor was 250 rpm; the feed rate was 10 kg / hour. The seal oil crude oil passes through the wiped film evaporator, the low boiling point components are evaporated, and the heavy oil phase components that have not been evaporated are collected to obtain refined seal oil.
Embodiment 3
[0039] Refined seal oil: containing OMEGA3 polyunsaturated fatty acid DPA 9.44%, EPA 12.52%, DHA 19.46% (percentage by weight), the sum of the three is 41.42%.
[0040] This refining seal oil is made by following method:
[0041] Equipment: same as embodiment one.
[0042] Raw material: with embodiment one.
[0043]Operating conditions: two-stage vacuum distillation is adopted, the pressure of the first polar molecular still is 2Pa, the evaporation temperature is 150°C, and the speed of the wiped film rotor is 100rpm; the pressure of the second polar molecular still is 0.2Pa, and the evaporation temperature is 300°C. The speed of the wiped film rotor was 250 rpm; the feed rate was 6 kg / hour. The seal oil crude oil passes through the wiped film evaporator, the low boiling point components are evaporated, and the heavy oil phase components that have not been evaporated are collected to obtain refined seal oil.
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