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54 results about "Ammonium lactate" patented technology
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This medication has 2 types of ingredients (emollient, keratolytic) that work together to treat or prevent dry, rough, scaly, itchy skin (e.g., eczema, keratosis, xerosis). Dry skin is caused by a loss of water in the upper layer of the skin. Emollients are substances that soften and moisturize the skin and decrease itching and flaking.
A method for recovery of highly pure alkyl lactate and lactic acid is provided, which includes a step 1 for producing source liquid comprising lactic acid or ammonium lactate; a step 2 for dehydrating the source liquid product of step 1; a step 3 for producing liquid mixture by sequentially adding and stirring alcohol and acid solution to the dehydrated source liquid; a step 4 for separating and removing ammonium salt precipitation from the liquid mixture of step 3; a step 5 for producing alkyl lactate from ammonium salt-free liquid mixture by esterification reaction; and a step 6 for separating alcohol and alkyl lactate by distillation from the mixture of step 5.
The invention discloses a moisturizing repair composition containing ceramide and phytosterol and a preparation method thereof and belongs to the field of cosmetics. The moisturizing repair composition is prepared from the following components in percent by mass: 0.01-5% of ceramide, 0.1-0.5% of phytosterol, 0.1-10% of shea butter, 0.5-10% of hydroxyethylurea, 0.1-6% of ammonium lactate, 1-30% ofa polyhydric alcohol moisturizing agent, 1-5% of an emulsifier, 1-20% of skin moistening grease, a proper amount of a thickener, essence and a preservative and the balance water, totaling 100%. The composition is an emulsified body which contains ceramide as the primary natural moisturizing factor of human skin and phytosterol and shea butter originated from plants, so that the composition has good moisturizing and repairing action, can keep the skin moisten and flexible and smooth, and can resist damage of outside severe climate environment to the skin.
A method for recovery of highly pure alkyl lactate and lactic acid is provided, which includes a step 1 for producing source liquid comprising lactic acid or ammonium lactate; a step 2 for dehydrating the source liquid product of step 1; a step 3 for producing liquid mixture by sequentially adding and stirring alcohol and acid solution to the dehydrated source liquid; a step 4 for separating and removing ammonium salt precipitation from the liquid mixture of step 3; a step 5 for producing alkyl lactate from ammonium salt-free liquid mixture by esterification reaction; and a step 6 for separating alcohol and alkyl lactate by distillation from the mixture of step 5.
Pharmaceutical, cosmetic and cosmeceutical compositions for topical application, containing, as an active ingredient, ammonium lactate and / or any other alpha-hydroxy carboxylic acid and / or salts thereof, processes of manufacturing these compositions and uses of these compositions in the treatment of medical and cosmetic conditions such as conditions associated with dry skin or scalp.
The invention discloses a technique that adopts ammonium lactate as raw material to make ethyl lacfate by rectifying. The adopted equipment includes rectifying tower, condenser on the top of tower and oil-water separator. It adopts metalhalide as catalyzer and place material mol proportion of ethanol and lactic acid being 1:1 and benzene being 30%-50% of lactic acidammonium weight. Its character: the temperature of the kettle of rectifying tower, 60-90 deg.C, that of the top of the tower, 60-70 deg.C, the pressure of the whole tower, normal, the top producing the azeotropic matter of ethanol, water and benzene, which enters into the separator through the condenser, the top of the separator set with liquid-flow mouth linked with the top of the tower, the reflux ratio, 0.5-2.0, the cleaned water at the bottom of the separator discharged outside, and the rectifying kettle producing it.
The invention provides a process for continuously producing L-ammonium lactate based on rhizopus sp., comprising the following steps. (1) Seed culture is processed, any kind of spore of rhizopus sp. is introduced to the seed culture medium to proceed aerobic liquid culture, the components of seed culture medium include carbon source, nitrogen source, inorganic salt and water, and the condensation of microcosmic salt in the seed culture medium is 0.8-1.2 grams every liter. (2) The product achieved by the step (1) is introduced to the fermentation culture medium to proceed aerobic liquid fermentation and culture, ammonia water or free ammonia enters in the fermentation process, the pH of the culture system is maintained to be 5 to 8, and then culture medium is fed-batch and the material is discharged, consequently the fermentation product is achieved, and then the target product of ammonium lactate is collected in the fermentation product. The invention has the advantages of simple operation, greatly reduced manufacture cost, easy separation of ammonium lactate form the fermentation liquid, and high recovery ratio.
The invention discloses a method for extracting and separating L-lactic acid from an ammonium lactate fermentation material liquid. The method comprises the following steps: (1) pre-treating the ammonium lactate fermentation material liquid; (2) carrying out sulphuric acidolysis on ammonium lactate; (3) adding an acidolysis material liquid and a coupling adsorbent in a centrifugal extractor respectively, and extracting L-lactic acid through coupling adsorption at 15-25 DEG C; (4) separating an organic phase from a water phase; and (5) adding the organic phase and hot water at 55-65 DEG C in the centrifugal extractor respectively, and extracting L-lactic acid through backcoupling adsorption. The method disclosed by the invention is capable of rapidly extracting and separating L-lactic acid from the lactic acid acidolysis liquid, changing the process route of separating various impurities from L-lactic acid one by one, and directly separating L-lactic acid through coupling adsorption by virtue of a coupling adsorption agent so as to leave the various impurities in a raffinate; because the coupling adsorption agent in the method disclosed by the invention has a specific adsorption property on L-lactic acid, the purpose of further purifying L-lactic acid is achieved, and a decolouring process and most of hybridization processes in the existing processes are removed.
The invention relates to a technology method for producing ethyl lactate from ammonium lactate. The technology method takes the ammonium lactate as a material and adopts enzymecatalysis for preparing the ethyl lactate and comprises the following steps of: adding the ammonium lactate and ethanol in a reactor, sequentially adding a solvent and an enzyme catalyst, wherein the mass proportioning ratio of the ammonium lactate to the ethanol is 1:3-11, the usage of the enzyme catalyst accounts for 14-29 percent of the mass of the ammonium lactate, and the adding quantity of the solvent in the ammonium lactate is 18-28.5ml / g; and sealing and putting the reactor in a constant temperature water bath shaker for reaction for 15-24 hours at temperature of 50-75 DEG C to obtain the ethyl lactate, wherein the enzyme catalyst is candida cylinder lipase, fuzzy humic mould lipase, candida antarcticalipase B or thermophilic fungi lipase. The method takes biological enzyme as a cytalyst and has the advantages of having moderate reaction conditions, being environment-friendly and the like, and the yield reaches over 30 percent; and the method omits lactate acidulating process of lactate salts, shortens the preparation process of the ethyl lactate and lowers the production cost of the ethyl lactate.
The ferricchloride modification ion exchange resin catalyst and the preparation method and application is provided, which relates to a catalyst and the preparation method and application. In order to solve the problem of the existing ammonium lactate catalyst with complicated preparation techniques, high production cost and low ammonium lactate catalyzing esterification efficiency. The catalyst is made of hydrogenous strong acid cation exchange resin and butanol solution of ferricchloride. The preparation method of the catalyst is realized by the following method: firstly, washing resin and drying; secondly, prepare compound resin; thirdly, proceed alcohol washing and acetone washing to compound resin and then dry, the ferricchloride modification ion exchange resin catalyst can be achieved. The catalyst is used in the ammonium lactate esterification reaction, which has simple preparation techniques, the cost is reduced by 5 to 8 per cent and the ammonium lactate esterification rate can reach 78 to 96 per cent.
Pharmaceutical, cosmetic and cosmeceutical compositions for topical application, containing, as active ingredients, urea and / or derivatives thereof and alpha-hydroxy acid and / or an ammonium salt thereof, such as ammonium lactate, processes of manufacturing same and use of same in the treatment of medical and cosmetic skin and scalp conditions.
A personal care composition having at least one hydroxyalkylurea (HAU) optionally in combination with at least one other moisturizing agent. The at least one HAU, alone or together with the at least one moisturizing agent, provides not only the perception of moisturization, but also actual increased moisturization efficacy. When the two are used in combination in a personal care composition, they are provided in a synergistically moisturizing effective ratio to provide that perception of moisturization and increased moisturization efficacy. Such personal care compositions provide an enhanced smooth feel as well as enhanced flexibility, elasticity, suppleness and firmness without leaving a heavy or greasy feel.
The invention discloses a heavy metalsoil remediation agent. The heavy metalsoil remediation agent is prepared from, by weight, 10-20 parts of edible fungus culture medium waste, 5-10 parts of urea,5-8 parts of starfish steroidal saponins, 2-8 parts of picfeltarraenin IA, 8-15 parts of vesica fusca sepiae, 2-5 parts of citronellal, 5-8 parts of maca, 2-6 parts of radix aconiti lateralis preparata, 2-6 parts of raspberry, 2-5 parts of carrot leaves, 1-3 parts of sugarbeet pulp, 1-3 parts of ammonium lactate, 1-3 parts of fulvic acid, 1-2 parts of additives and 60-100 parts of water. The heavy metalsoil remediation agent is capable of effectively reducing the content of cadmium in an aboveground portion and an underground portion and has great heavy metal contamination treatment effects;by adoption of the edible fungus culture medium waste as a raw material, the utilization rate of the edible fungus culture medium waste is increased, and waste recycling is realized, so that energy saving and environmental friendliness are realized.
The invention relates binary catalysissystem and its application in ammonlum lactate esterification reaction, and the method for preparation of magnetismsolid acid catalyst in the said catalysissystem. It solves the problem of magnetismsolid acid catalyst not suiting ammonlum lactate esterification. In the invention the binary catalysissystem comprises the magnetismsolid acid catalyst and tin dichloride, the proportion by weight of which is 20: 1-1: 20. The method for making magnetism solid acid catalyst comprises the following steps: 1. adding ammonia into ferricpersulfate solution; 2. solid-liquid separation, drying and powdering the solid; 3.adding the powder into the nickelsulfate solution; 4. evaporating to dryness and roasting; 5. cooling. The said catalysis system is used in ammonlum lactate esterification reaction, comprising the following proportion: a. the mass ratio of ammonium lactate and the C1-C4 alcohol being 10í†1-1í†10; b. the weight ratio of catalysis system and ammonium lactate being 0.005-5úÑ, and the magnetism solid acid catalyst and tin dichloride being 20í†1-1í†20; c. the esterification reaction reacting in atmosphere pressure, at 115-140íµ, for 3.5-11h. The invention has good selectivity, adapted for ammonlum lactate esterification reaction.
The invention belongs to the technical field of pharmaceutical and chemical engineering, and relates to a preparation method of ammonium lactate solids, in particular to a method for changing an ammonium lactate solution into the ammonium lactate solids. The preparation method of the ammonium lactate solids mainly comprises steps as follows: 1) preparation of the ammonium lactate solution : a lactic acid solution reacts with ammonia water to produce the ammonium lactate solution; 2) preparation of a concentrated ammonium lactate solution : the ammonium lactate solution is extracted with acetonitrile and concentrated, and the concentrated ammonium lactate solution is obtained; 3) preparation of the ammonium lactate solids: the concentrated ammonium lactate solution is dissolved in ethanol, acetonitrile, acetone or a acetonitrile and acetonemixed solution is added, and the solids are precipitated. The ammonium lactate solid products prepared with the preparation method of the ammonium lactate solids are high in purity, good in stability, easy to store and transport and suitable for mass industrial production.
The invention provides a self-induction-based method for biomimetic titanification of immobilized protease. Immobilization of the protease is achieved in the induced biomimetic titanification process by using the inductive effect of papain on biomimetic titanification of a titanium precursor dihydroxy bis(ammonium lactate) titanium to obtain the immobilized protease employing titaniumoxide as a carrier. The defects that a traditional immobilization method is complicated in immobilization process, the immobilized protease is poor in biocompatibility of an enzyme and the carrier, relatively weak in bonding action with the carrier, poor in stability and short in service life, and the immobilization reaction is relatively violent and easily causes enzyme inactivation and activity reduction are overcome, and the method has the advantages of being simple in immobilization process, mild in condition, high in efficiency, good in enzymerecovery rate of the immobilized protease and good in embedding rate.
The invention belongs to the technical field of skin care and health care products, particularly relates to a sustained-release microcapsule wrapping traditional Chinese medicine extract and a preparation method and application thereof, and solves the problems that in the prior art, the traditional Chinese medicine extract is directly added into a skin care product to be mixed and emulsified for use, due to the special chemical structure of traditional Chinese medicine active ingredients, the biological activity on the skin surface is extremely easy to lose, the active ingredients cannot reach the deep layer of the skin, cannot repair the skin barrier and cannot achieve a remarkable skin care effect. The sustained-release microcapsule wrapping the traditional Chinese medicine extract comprises a capsule core material and a capsule material wrapping the capsule core material; the capsule core material is prepared by mixing and compounding a traditional Chinese medicine extract, ascorbyl palmitate and xylitolfatty acid ester; the capsule material is prepared by mixing and compounding fatty acidsucrosepolyester, ammonium lactate, hydroxy propyl distarch phosphate and ethyl p-hydroxybenzoate. The microcapsule can effectively ensure that the active ingredients of the traditional Chinese medicines can abut against the deep layer of the skin and are slowly released, thereby playing a role in repairing the skin barrier.