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52results about How to "Fast digestion" patented technology

Pretreatment method for determining multiple heavy metal elements in soil simultaneously

The invention discloses a pretreatment method for determining multiple heavy metal elements in soil simultaneously. The pretreatment method comprises steps as follows: step (1): sample weighing: the soil is air-dried, ground and screened with a nylon sieve, a soil sample is weighed and put into a microwave digestion tube through a polytetrafluoroethylene long-neck funnel, and the funnel is slightly flapped before the funnel is removed so that all the soil sample attached to the wall of the funnel enter the digestion tube; step (2): digestion: nitric acid, hydrochloric acid and hydrofluoric acid are added to the digestion tube, a cover is screwed down, and the digestion tube is put into a microwave digestion instrument for digestion; step (3): acid driving: after microwave digestion is finished, hydrogen peroxide is added to the digestion tube; then the microwave digestion tube is put into a temperature-controlling acid driver in a fume cupboard for direct acid driving until the volume is smaller than 1 mL, then a solution is directly transferred to a volumetric flask, the volume is constant, and a to-be-tested solution is obtained. With the adoption of the pretreatment method, the digestion speed of the sample can be increased, the pre-treatment step of the sample is simplified, and the accuracy of the detection analysis result is guaranteed.
Owner:PUER COMPREHENSIVE TECHN TESTING CENT

High-volume phosphogypsum composite stable roadbed material and preparation method thereof

The invention discloses a high-volume phosphogypsum composite stable roadbed material and a preparation method thereof, and belongs to the technical field of highway construction materials. The roadbed material comprises the following components by weight percentage: 90-95% of phosphogypsum, 1-6% of a curing agent, 1.5-4% of a curing accelerator and 2-4% of water; the curing agent comprises Portland cement, superfine steel slag powder and blast furnace slag powder; the curing accelerator comprises water glass and a cationic styrene-acrylic emulsion. Through the synergistic effect of all the components of the curing accelerator, soluble P and F in the phosphogypsum can be effectively cured, early hydrolysis is promoted, the gelling activity of the phosphogypsum with the Portland cement andthe like is enhanced, an electronegative product generated in the modification process can be chemically bonded with cationic styrene-acrylic emulsion, the binding power between the raw materials is enhanced, and the mechanical strength of the material is improved; and secondly, under the bridging action of the electronegative product, the cationic styrene-acrylic emulsion can be firmly coated onthe surface of the phosphogypsum and the like to prevent the phosphogypsum from being dissolved in water, thereby enhancing the water stability.
Owner:中南安全环境技术研究院股份有限公司

Method for detecting molybdenum element in milk powder

The invention relates to a method for detecting molybdenum element in milk powder. The used equipment is an inductively coupled plasma atomic emission spectrometer. The method has the following steps of: 1) preparing molybdenum element standard solution and making a standard curve according to the standard solution; 2) oxidizing a milk powder sample to be tested by using peroxide, performing acid treatment by using nitric acid, digesting in a microwave digestion system, and detecting by using equipment parameters same as the standard solution to obtain a detection result of the sample to be tested; and 3) comparing the detection result of the sample to be tested with the standard curve to determine the content of the molybdenum element in the sample to be tested. The instrument detection limit of the method is 0.0071 mu g/ml, and in an element linear range, the related coefficient r is over 0.999, and the recovery rate is 92.0 to 101.8 percent. The method can quickly and accurately detect the content of the molybdenum element in the milk powder, and has the advantages of low element loss and pollution probability in the sample preparing process, accurate and reliable result, good repeatability and high sensitivity.
Owner:INNER MONGOLIA MENGNIU DAIRY IND (GRP) CO LTD

Dendrobium officinale and yeast protein powder mixed feed capable of increasing goose weight gain rate and nutrition absorption rate and preparation method of feed

The invention discloses a dendrobium officinale and yeast protein powder mixed feed capable of increasing the goose weight gain rate and the nutrition absorption rate and a preparation method of the feed. The method comprises the steps that corn is adopted as the main material which is assisted with ferrous bisglycinate, radix polygoni multiflori powder, glutamine dipeptide, puffing cow blood meal, dried tangerine peel powder, aloe oil and the like, modification treatment is conducted on the corn, the goose weight gain rate and the nutrition absorption rate the can be increased, the appetite of geese is promoted, the digestive function of the geese is enhanced, and growth and development of the geese are promoted; dendrobium officinale and yeast protein powder are matched with each other synergistically, growth and weight gain of the geese can be rapid, and the feed utilization ratio is increased; by means of matching of defatted fish meal, riboflavin and papaya protein powder, uniform dispersion of all nutrient substances in the geese is promoted, and full absorption is achieved; by means of addition of pickle juice and leaves of toona sinensis, the digestive function of the geese can be improved, and intestinal health of the geese is promoted.
Owner:ANHUI YUNJIN AGRI SCI & TECH DEV CO LTD

Pre-processing method of rubber material element detection

The invention provides a pre-processing method of rubber material element detection. The method comprises steps that: A, a sample preparation step is carried out, wherein a small block of rubber sample is crushed into powder; B, a sample digestion step is carried out, wherein a small amount of rubber powder sample is placed in a polytetrafluoroethylene microwave digestion tank, concentrated nitric acid and concentrated hydrochloric acid are added into the tank, and the materials are stood; C, the polytetrafluoroethylene microwave digestion tank is adopted as a main controlling tank, microwave digestion program parameters are configured, and microwave digestion is carried out; D, when the microwave digestion program is finished, the material is cooled to room temperature, such that a completely digested solution of the rubber sample is obtained, and the rubber sample pre-processing procedure is finished. With the method provided by the invention, a polytetrafluoroethylene digestion tank explosion phenomena is avoided; uncontrollable losses of certain elements when rubber samples are processed through a high-temperature ashing method are avoided; the operation procedure is simple, the digestion speed is fast, and pre-processing cost is saved; and the digested solution is clear, such that confounding factors during a determination procedure are reduced.
Owner:SHANGHAI FALAB TEST

Method for detecting COD content in water by instrument

The invention, which relates to the technical field of COD content detection, discloses a method for detecting the COD content in water by an instrument. The method comprises the following steps that:step one, test building is performed; to be specific, an instrument detects the COD content in water by using a measuring method that uses potassium dichromate as an oxidant, silver sulfate as a catalyst, a mercury sulfate as a masking agent for chloride ions and measurement of a COD digestion system as the base under the acidic condition of sulfuric acid; step two, a rapid digestion spectropho-tometry method is performed; to be specific, a sealing tube is used as a digestion tube, a small number of water samples and reagents are placed in the sealing tube, the sealing tube is placed in a small constant-temperature heating container and then constant-temperature heating and digestion are performed, and a COD value is determined by the spectrophotometry method. According to the invention,the method has advantages of small occupied space, low energy consumption, and small reagent amount and the like; defects of large equipment occupied space, high energy consumption, and large reagentdosage of the existing COD content detection method are overcome; and problems are solved by the method for detecting the COD content in water by an instrument.
Owner:CHENGYU VANADIUM TITANIUM TECH CO LTD

RNA extraction kit suitable for normal-temperature transportation, and extraction method

The invention relates to an RNA extraction kit suitable for normal-temperature transportation. The kit comprises a lysis binding solution, and the lysis binding solution contains guanidine isothiocyanate with the concentration of 1 to 5 M, sodium thiocyanate with the concentration of 0.2 to 3 M, trihydroxymethyl aminomethane with the concentration of 0.01 to 0.1 M, tetrasodium iminodisuccinate with the concentration of 0.001 to 0.05 M, sodium ascorbate with the mass fraction of 0.05-1%, betaine with the mass fraction of 0.1-2%, Tween 20 with the mass fraction of 1-6%, sodium acetate with the concentration of 0.05 to 0.5 M, and isopropanol withthe mass fraction of 25-55%. The lysis binding solution does not contain toxic organic solvents such as phenol and does not contain reagents such as protease K needing cold-chain transportation, so that the RNA extraction kit can be transported under the condition of normal temperature. The lysis binding solution has the effects of lysis of cells / viruses and promotion of combination of nucleic acid and magnetic beads, can complete lysis and combination in one step, and is more suitable for an automatic nucleic acid extractor. The two protein denaturants are combined for use, and compared with single use of one protein denaturant, the capacity of removing impurities such as protein with complex chemical properties can be enhanced.
Owner:苏州赛普生物科技股份有限公司

Determination method for chromium content of inhalable particles in soil dust and detection method

The invention discloses a determination method for the chromium content of inhalable particles in soil dust. The determination method includes the following steps of sample extraction, sample pretreatment, acid removal and volume metering, preparation of a standard blank solution and a standard working solution, and graphite furnace atomic absorption spectrometry determination. The invention further discloses a detection method for the accuracy of the determination method for the chromium content of inhalable particles in soil dust. The detection method includes the following steps that a national standard substance with the known chromium content is prepared into five parts of sample solutions to be detected, wherein the concentrations of the sample solutions to be detected are different; the chromium content in each sample solution to be detected is detected with the determination method for the chromium content of inhalable particles in soil dust so that the precision of the determination method for the chromium content of inhalable particles in soil dust can be verified. The determination method and the detection method have the advantage that sampling time is short, digestion is fast, little interference exists in determination, and the result is accurate and reliable.
Owner:SHANDONG UNIV OF SCI & TECH

Resource-saving low-carbon cement clinker and preparation method thereof

The invention discloses a resource-saving low-carbon cement clinker and a preparation method thereof, and belongs to the technical field of Portland cement clinker production. The cement clinker comprises the following raw materials in percentage by mass: 45-70% of high-calcium low-magnesium limestone, 10-40% of barren rock, 4-12% of shale or sandstone, 4-12% of slag, 1-3% of sulfate slag or iron slag, 1-3% of fly ash, 0-3% of coal cinder or coal gangue, 0.5-3% of phosphorus slag and phosphogypsum and 0.1-0.3% of an added activating agent. According to the resource-saving low-carbon cement clinker and the preparation method thereof of the invention, a large amount of solid waste is utilized, the adopted industrial waste residue is formed by high-temperature calcination, carbonate hardly exists, and CO2 hardly occurs after high-temperature calcination is performed again; the mixing amount of the industrial waste residues is high, the use amount of limestone is greatly reduced; the mineralization of trace elements in the industrial waste residues is utilized, and the activating agent is added, so that the burnability of the raw materials is improved, the sintering stability of the clinker is reduced, and the performance of the clinker is improved; the firing temperature of the low-carbon cement clinker is reduced by 100-150 DEG C compared with the firing temperature 1450 DEG C of traditional Portland cement clinker, and therefore, the coal consumption is obviously reduced, and the emission of CO2 is reduced.
Owner:阳新娲石水泥有限公司

Effervescent tablets for effectively relieving labor pains

The present invention discloses effervescent tablets for effectively relieving labor pains, more particularly discloses the effervescent tablets which can quickly replenish energy, relieve fatigues, relieve maternal anxiety, irritability, tension and other bad mood and pains, and belongs to the technical fields of solid drink and special dietary edible food processing. The effervescent tablets are characterized by consisting of the following components in mass percentages: 25-35% of crystalline fructose, 5-15% of xylitol, 20-30% of sodium bicarbonate, 25-35 % of citric acids, 2.5-5% of medium chain triglycerides, 0.5-5% of gamma-aminobutyric acids, 0.4-4% of tea leaf theanine, 0.11-0.14% of taurine, 0.0022-0.008% of pantothenic acid, 0.0009-0.0022% of vitamin B1, 0.0009-0.0022% of vitamin B2, 0.0009-0.0022% of vitamin B6, 1-5% of an adhesive, and 0.1-0.5% of a lubricant. The advantages and beneficial effects are that the present invention also prepares the effervescent tablets which are good in stability, short in disintegration time, and strong in interestingness. The effervescent tablets can rapidly form even solution in water, can be consumed in an oral and sucking manner, can also be chewed, are easy to take, at the same time combine the both advantages of the tablets which are convenient for storage and carrying, can be consumed normally, and will not bring harms, and toxic and side effects to the body.
Owner:李卫平

Curing agent for mud hardening treatment of empty pile section, preparation method and construction method

The invention relates to the technical field of mud hardening treatment of an empty pile section, and discloses a curing agent for mud hardening treatment of an empty pile section, a preparation method and a construction method. The curing agent includes an efficient structural agent and an admixture. The efficient structural agent and the admixture are blended with water to form curing slurry. The efficient structural agent is stirred, then the admixture is added and stirred, then water is added and the mixture is stirred to form the curing slurry, achieving preparation. Through multi-stage stirring, cured bodies and water are mixed more thoroughly; conveying compressed air and curing slurry to the empty pile section so that the curing slurry and waste mud are stirred and mixed, achievinghardening treatment. Through multi-stage stirring, components of the curing agent are mixed more thoroughly. By adoption of the curing agent, the hydration reaction degree is higher, the curing speedis higher, high-water-content mud in construction can be consumed rapidly, hidden safety risks caused by long-term stacking can be prevented, efficient resource utilization is achieved, and strengthof cured soil is higher and meets the bearing capacity of foundation soil.
Owner:SHENZHEN HONGYEJI GEOTECHNICAL TECH CO LTD

Method for jointly measuring phosphorus in soil by high-pressure digestion and inductively coupled plasma spectrometer

The invention provides a method for jointly measuring phosphorus in soil through high-voltage digestion and an inductively coupled plasma spectrometer, and relates to the technical field of environmental monitoring. According to the method, the high-pressure digestion and the inductively coupled plasma spectrometer are combined to determine the content of phosphorus in the soil. According to the invention, the digestion process is carried out in a pressure cooker, the high-pressure digestion has the advantages of high digestion speed, controllable reaction temperature and reaction time, no need of personnel on duty, low operation difficulty and difficulty in phosphorus loss under closed conditions, and the accuracy of a measurement result is improved while the operation is simple and convenient; the digestion process is carried out in a closed container, so that toxic and harmful substances cannot be released due to the reaction between the soil and aqua regia, and the harm to analystsand the environment can be effectively avoided. The calibration curve used in the method is a working curve, and compared with a standard curve, the interference of a matrix on an analysis result canbe effectively avoided, so that a measured value is closer to a true value.
Owner:黄麟杰

Rapid harmless emergency treatment method of enteromorpha

The invention discloses a rapid harmless emergency treatment method of enteromorpha. The rapid harmless emergency treatment method of enteromorpha comprises the following steps of 1, collecting enteromorpha, 2, transporting the collected enteromorpha to an emergency storage, 3, carrying out aerobic composting treatment on the collected enteromorpha, and 4, carrying out emergency landfill treatment on the enteromorpha which is not subjected to the aerobic composting treatment, wherein the emergency landfill treatment comprises the following steps of A, carrying out seepage prevention treatmenton the bottom of an emergency landfill through the processes of orderly laying a clay membrane lower seepage-proof protection layer, a high-density polyethylene (HDPE) geomembrane and a nonwoven geotextile membrane upper protection layer on a base of the emergency landfill, B, transporting enteromorpha to the emergency landfill, and laying an enteromorpha layer on the emergency landfill subjectedto the seepage prevention treatment, and C, carrying out closure covering treatment on the enteromorpha layer. In the invention, aerobic composting treatment on enteromorpha needs low costs of capital construction and operation; an end product is compost; and resource recovery is realized. The rapid harmless emergency treatment method of enteromorpha can carry out simple and efficient emergency landfill treatment in the case of insufficient enteromorpha aerobic treatment capabilities, combines with aerobic composting treatment on enteromorpha, and is very suitable for emergency treatment carried out in large-scale outbreak of algae such as enteromorpha and the like.
Owner:青岛市环境卫生科研所
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