Rare-earth fluorescent material prepared in vertical electric furnace and preparing method thereof
A technology of rare earth fluorescent material and electric furnace, which is applied in the field of rare earth fluorescent material and its preparation, and can solve the problem of high production cost
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Embodiment 1
[0017] Embodiment 1, a kind of rare earth fluorescent material prepared by a vertical electric furnace of the present invention, it is based on aluminum oxide, aluminum hydroxide, thallium trioxide, and yttrium trioxide as main raw materials, and cerium Diboron oxide and niobium pentoxide are trace additives, each component is weighed according to the following parts by weight, take aluminum oxide 21, aluminum hydroxide 30, dithallium trioxide 13, diyttrium trioxide 36, dioxide Cerium 0.1, diboron trioxide 1.5, niobium pentoxide 0.5, mix the above weighed components and ball mill for 5 to 20 hours, then put the ball milled mixture into a special cylindrical burning bowl for vertical electric furnace, The inside of the cylindrical burning bowl is covered with another small burning bowl, carbon powder is put into it, heat treated at 1300-1600°C for 2-8 hours, after cooling, the rare earth fluorescent material is obtained through powder selection and sieving.
[0018] When the fi...
Embodiment 2
[0019] Embodiment 2, a kind of rare earth fluorescent material prepared by vertical electric furnace of the present invention, it is main raw material with aluminum oxide, aluminum hydroxide, dithallium trioxide, diyttrium trioxide, with cerium oxide, three Diboron oxide and niobium pentoxide are trace additives, each component is weighed according to the following parts by weight, take aluminum oxide 24, aluminum hydroxide 30, dithallium trioxide 16, diyttrium trioxide 30, dioxide Cerium 0.1, diboron trioxide 1.5, niobium pentoxide 0.5, mix the above weighed components and ball mill for 5 to 20 hours, then put the ball milled mixture into a special cylindrical burning bowl for vertical electric furnace, The inside of the cylindrical burning bowl is covered with another small burning bowl, carbon powder is put into it, heat treated at 1300-1600°C for 2-8 hours, after cooling, the rare earth fluorescent material is obtained through powder selection and sieving.
[0020] When th...
Embodiment 3
[0021] Embodiment 3, a rare earth fluorescent material prepared by a vertical electric furnace according to the present invention, which uses aluminum oxide, aluminum hydroxide, thallium trioxide, and yttrium trioxide as main raw materials, and cerium oxide, three Diboron oxide and niobium pentoxide are trace additives, each component is weighed according to the following parts by weight, take aluminum oxide 40, aluminum hydroxide 15, dithallium trioxide 30, diyttrium trioxide 15, dioxide Cerium 0.1, diboron trioxide 1.5, niobium pentoxide 0.5, mix the above weighed components and ball mill for 5 to 20 hours, then put the ball milled mixture into a special cylindrical burning bowl for vertical electric furnace, The inside of the cylindrical burning bowl is covered with another small burning bowl, carbon powder is put into it, heat treated at 1300-1600°C for 2-8 hours, after cooling, the rare earth fluorescent material is obtained through powder selection and sieving.
[0022] ...
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