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Rare-earth fluorescent material prepared in vertical electric furnace and preparing method thereof

A technology of rare earth fluorescent material and electric furnace, which is applied in the field of rare earth fluorescent material and its preparation, and can solve the problem of high production cost

Inactive Publication Date: 2009-04-01
XIAMEN QUANTUM STAR TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the existing rare-earth fluorescent materials that can be combined with light-emitting diodes to form white light have high production costs and certain limitations in technology.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] Embodiment 1, a kind of rare earth fluorescent material prepared by a vertical electric furnace of the present invention, it is based on aluminum oxide, aluminum hydroxide, thallium trioxide, and yttrium trioxide as main raw materials, and cerium Diboron oxide and niobium pentoxide are trace additives, each component is weighed according to the following parts by weight, take aluminum oxide 21, aluminum hydroxide 30, dithallium trioxide 13, diyttrium trioxide 36, dioxide Cerium 0.1, diboron trioxide 1.5, niobium pentoxide 0.5, mix the above weighed components and ball mill for 5 to 20 hours, then put the ball milled mixture into a special cylindrical burning bowl for vertical electric furnace, The inside of the cylindrical burning bowl is covered with another small burning bowl, carbon powder is put into it, heat treated at 1300-1600°C for 2-8 hours, after cooling, the rare earth fluorescent material is obtained through powder selection and sieving.

[0018] When the fi...

Embodiment 2

[0019] Embodiment 2, a kind of rare earth fluorescent material prepared by vertical electric furnace of the present invention, it is main raw material with aluminum oxide, aluminum hydroxide, dithallium trioxide, diyttrium trioxide, with cerium oxide, three Diboron oxide and niobium pentoxide are trace additives, each component is weighed according to the following parts by weight, take aluminum oxide 24, aluminum hydroxide 30, dithallium trioxide 16, diyttrium trioxide 30, dioxide Cerium 0.1, diboron trioxide 1.5, niobium pentoxide 0.5, mix the above weighed components and ball mill for 5 to 20 hours, then put the ball milled mixture into a special cylindrical burning bowl for vertical electric furnace, The inside of the cylindrical burning bowl is covered with another small burning bowl, carbon powder is put into it, heat treated at 1300-1600°C for 2-8 hours, after cooling, the rare earth fluorescent material is obtained through powder selection and sieving.

[0020] When th...

Embodiment 3

[0021] Embodiment 3, a rare earth fluorescent material prepared by a vertical electric furnace according to the present invention, which uses aluminum oxide, aluminum hydroxide, thallium trioxide, and yttrium trioxide as main raw materials, and cerium oxide, three Diboron oxide and niobium pentoxide are trace additives, each component is weighed according to the following parts by weight, take aluminum oxide 40, aluminum hydroxide 15, dithallium trioxide 30, diyttrium trioxide 15, dioxide Cerium 0.1, diboron trioxide 1.5, niobium pentoxide 0.5, mix the above weighed components and ball mill for 5 to 20 hours, then put the ball milled mixture into a special cylindrical burning bowl for vertical electric furnace, The inside of the cylindrical burning bowl is covered with another small burning bowl, carbon powder is put into it, heat treated at 1300-1600°C for 2-8 hours, after cooling, the rare earth fluorescent material is obtained through powder selection and sieving.

[0022] ...

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PUM

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Abstract

The RE fluorescent material in vertical electric furnace is prepared with Al2O3, Al(OH)3, Tl2O3 and Y2O3 as main material, and CeO2, B2O3 and Nb2O5 as micro additives in certain weight proportion, and through mixing, ball milling for 5-20 hr, setting the milled mixture inside one special cylindrical baking pot with one small backing pot holding carbon powder inside it, heat treatment at 1300-1600 deg.c inside vertical electric furnace for 2-8 hr, cooling, sorting and sieving to obtain the RE fluorescent material. The said preparation process can produce white RE fluorescent material capable of matching LED in industrial scale and in low cost.

Description

technical field [0001] The invention relates to a rare earth fluorescent material and a preparation method thereof, in particular to a rare earth fluorescent material prepared by a vertical electric furnace and a preparation method thereof. Background technique [0002] Since ancient times, human beings have loved light and feared darkness. Edison's invention of the light bulb has brought light to human beings, enabling people to work, study and live at night as in daytime. The advent of fluorescent lamps has greatly improved the lighting industry. Great development, the invention of rare earth energy-saving lamps, is known as a new milestone for human civil lighting sources. Among many practical luminescent materials that humans have developed, rare earth elements play a great role, and the role of rare earth elements far exceeds that of other elements. . In fact, the phenomenon of material luminescence can be roughly divided into two categories: one is that the material i...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K11/78
Inventor 熊兆贤熊宏鑫
Owner XIAMEN QUANTUM STAR TECH
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