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Preparation process and application of perfumery nano capsule dispersant liquid

A nanocapsule and dispersion technology, which is applied in microcapsule preparation, microsphere preparation, essential oil/spice, etc., can solve the problems of easy friction and slip, easy washing, easy blocking of mesh holes, etc., and achieves the effect of good processing performance.

Inactive Publication Date: 2010-09-29
常州汉诺斯生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved in the present invention is: to solve the problem that the existing spice capsules are used as fragrance microcapsules in the fragrance processing of textiles, because the particles are too large, and the mesh holes are easily blocked during printing; Fabrics or other solid surfaces are not only easy to rub and slip off but also easy to wash off, and cannot achieve long-lasting fragrance and other technical problems. The fragrance nanocapsule prepared by the preparation method of the fragrance nanocapsule dispersion of the present invention is a spherical capsule. , containing essence, the average particle diameter is about 140-180nm, the capsule wall has thermosetting properties, strong, and good processing performance

Method used

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  • Preparation process and application of perfumery nano capsule dispersant liquid
  • Preparation process and application of perfumery nano capsule dispersant liquid
  • Preparation process and application of perfumery nano capsule dispersant liquid

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Preparation of lavender spice nanocapsule dispersion:

[0032] Homogenize 50 parts of lavender essence, 15 parts of dispersing emulsifier, and 300 parts of distilled water in a high-shear mixing emulsifier at a high speed at a speed of 10,000 rpm. After 30 minutes, adjust the pH to 2.5 to 3.5 with acetic acid, and then homogenize The emulsion was poured into a three-necked flask and placed in a constant temperature water bath. Under stirring conditions and a stirring speed of 300rpm, 80 parts of etherified melamine resin prepolymer was added dropwise, and the temperature was raised to 60°C. Wall; after cooling the system to room temperature, add 80 parts of etherified melamine resin prepolymer dropwise under stirring condition, raise the temperature to 70°C, keep it warm, and carry out the second wall building. Cool and neutralize to pH=7 to obtain a lavender nanocapsule dispersion. Gained fragrance nanocapsule electron micrograph is shown in figure 1 .

Embodiment 2

[0034] Scent finishing of colored cotton knitted fabrics:

[0035] Process: padding method: padding (two dipping and two rolling, liquid carrying capacity 70%) → drying (90-100°C)

[0036] Padding solution prescription:

[0037] Lavender essence nanocapsule dispersion 50g / L

[0038] Formaldehyde-free super soft adhesive 30g / L

[0039] The color of the colored cotton fabric before and after fragrance finishing is basically the same, and the hand feeling has little change. The formaldehyde content is 5.3mg / kg. After the colored cotton knitted fabric is washed 20 times, the fragrance content in the fabric only decreases by about 29%. The fabrics treated with fragrance nanocapsules were stored openly, and as the storage time prolongs, the fragrance content on the fabrics decreases continuously, see figure 2 Shown, to 6 months, still have the essence of 450mg / Kg to remain in the capsule of fabric, and fabric sends out pleasant fragrance.

Embodiment 3

[0041] Preparation of Baiaishen essence nanocapsule dispersion:

[0042] Homogenize 30 parts of Baiaishen essence, 10 parts of anionic dispersant, 5 parts of nonionic emulsifier, and 300 parts of distilled water in a high-shear mixing emulsifier at a high speed. The homogenization rate is 10,000 rpm. After 30 minutes, adjust with acetic acid The pH is 3-4, then pour the homogenized emulsion into a three-necked flask, put it into a constant temperature water bath, and under stirring conditions, at a stirring speed of 300rpm, add 80 parts of etherified melamine resin prepolymer dropwise, and heat up To 56°C, keep it warm for 2 hours to build a single-layer wall; after cooling the system to room temperature, add 80 parts of etherified melamine resin prepolymer dropwise under stirring conditions, raise the temperature to 70°C, keep it warm, and carry out the second wall build . Cool and neutralize to pH=7 to obtain Baiaishen essence nanocapsule dispersion.

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Abstract

The present invention relates to fine chemical technology, and is especially preparation process and application of nanometer perfume capsule dispersing liquid. Etherified melamine resin prepolymer is used as the monomer for forming capsule wall material and is in-situ polymerized to prepare nanometer perfume capsule dispersing liquid. The said process can prepare capsule with concentrated particle size, average particle size of 140-180 nm, excellent dispersivity and excellent slow releasing property, and the capsule may be used in the scenting finishing of fabrics as well as ink, paint, printed matter, etc.

Description

technical field [0001] The invention belongs to the technical field of fine chemicals, and in particular relates to a preparation method and application of a spice nanocapsule dispersion. Background technique [0002] Capsules are classified according to particle size: large capsules, with a particle size greater than 1,000 μm; microcapsules, with a particle size in the range of 1 to 1,000 μm; and nanocapsules, with a particle size of less than 1 μm. In the 21st century, people are aware of the efficacy of microcapsule finishing, especially in developed countries, such as Japan, the United States and some European countries. The rapid development of microcapsule technology has led to technological innovation in textiles in terms of functionality, fashion, and advancement. Fragrance It can not only make people have beautiful reverie, but also has many health care effects. Scientific research has proved that many aromatics have the effects of calming, sterilizing, and health ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B9/00B01J13/18
Inventor 纪俊玲苏东震
Owner 常州汉诺斯生物科技有限公司
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