Ampere type humidity sensing device
A technology of humidity sensing and humidity sensor, applied in the field of electrochemistry, can solve the problems of nonlinear range of response signal, high instrument cost, poor anti-interference, etc., and achieve the effect of strong anti-interference, simple equipment and convenient production
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Embodiment 1
[0041] Preparation of 1-ethyl-3-methylimidazolium bromide
[0042] Under room temperature and stirring conditions, 9.1ml of bromoethane (0.126mol) was slowly added dropwise to 10ml of N-methylimidazole. After 24h, it was washed with ethyl acetate three times, filtered, and vacuum-dried. Reaction equation:
[0043]
Embodiment 2
[0045] Preparation of [1-ethyl-3-methylimidazole][tetrafluoroboric acid] ionic liquid
[0046] Under the conditions of room temperature and rapid stirring, the HBF 4 Acid (15.2cm 3 0.116mol) Slowly add Ag 2 O slurry (13.49g 0.058molAg 2 O dissolved in 50cm 3 water), stir quickly. The reaction vessel was wrapped with aluminum foil to prevent light fall. Stir for another 1 h until Ag 2 O reacted completely to give a colorless solution. Add 22.24g 0.116mol of 1-ethyl-3-methylimidazolium inner salt obtained in Example 1, stir at room temperature for 2h, filter and separate. At 70°C, vacuum-dried, the product was a white liquid. The reaction equation is:
[0047]
Embodiment 3
[0049] Preparation of 1-butyl-3-methylimidazolium bromide
[0050] Under stirring at room temperature, slowly drop 6.46ml of n-bromobutane (0.06mol) into 4.76ml of N-methylimidazole. After 24h, wash with ethyl acetate three times. Filter and dry in vacuo. The reaction equation is:
[0051]
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