Photosensitive resin composition
A resin composition and photosensitivity technology, applied in optics, photosensitive materials for optomechanical equipment, optomechanical equipment, etc., can solve the problem of film remaining rate decrease, achieve excellent performance, low dielectric constant, coating Excellent effect
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[0073] Hereinafter, although an Example demonstrates this invention more concretely, the form of this invention is not limited to these Examples.
Synthetic example 1
[0074] Synthesis Example 1 (Synthesis of Acrylic Copolymer 1)
[0075] In a 2000ml four-necked flask equipped with a stirrer, a condenser tube, a thermometer, and a nitrogen inlet tube, add 700 g of propylene glycol monomethyl ether acetate, 171 g of methyl methacrylate, 90 g of 2-hydroxypropyl methacrylate, and Acrylic acid 39g, dimethyl-2,2'-azobis (2-methylpropionate) 8.0g, and stirred, while nitrogen gas was passed through, the temperature was raised, and polymerized at 85°C for 8 hours to obtain heavy Acrylic copolymer 1 with an average molecular weight of 21,000.
Embodiment 1
[0077] 100 parts by weight of the acrylic copolymer 1 prepared in Synthesis Example 1, 25 parts by weight of an ester compound represented by the following formula (V) (the esterification rate is 50%), and 5 parts by weight of the phenolic compound represented by the above formula (III) Compound, 17 parts by weight of epoxy group-containing curing agent Techmoa VG3101L (produced by Mitsui Chemicals (KK)) and 0.5 parts by weight of monooctyl maleate are dissolved in propylene glycol monomethyl ether acetate / diglyme ( 80 / 20), in order to prevent radial creases on the resist film during spin coating, that is, so-called striations, 300 ppm of fluorine-based surfactant Megafac R-08 (manufactured by Dainippon Inki Chemical Industry Co., Ltd.) was further added. ), and stirred, and then filtered through a 0.2 μm filter to prepare the photosensitive resin composition 1 of the present invention.
[0078]
[0079]
[0080] The photosensitive resin composition 1 prepared above was spi...
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Abstract
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