Method for synthesizing castor oil polyoxyethylene ether
The technology of a polyoxyethylene ether and a synthesis method is applied in the synthesis field of organic compounds, and can solve the problems such as few reports of the synthesis method, and achieve the effects of low equipment requirements, high yield and light color and luster.
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Example Embodiment
[0010] Embodiment 1: add 600g castor oil and 1.1g powdery sodium methoxide in the reaction kettle, be warming up to 130 ℃, after vacuum dehydration 1 hour, add ethylene oxide 109g, after 150 ℃ of reaction is complete, be cooled to 80 ℃ out. material. The test data of this experimental product are: hydroxyl value of 137.7 and molecular weight of 1100.
Example Embodiment
[0011] Embodiment 2: add 400g castor oil and 1.1g solid KOH in the reaction kettle, be warming up to 130 ℃, after vacuum dehydration 1 hour, add ethylene oxide 1032g, after 150 ℃ of reaction is complete, be cooled to 80 ℃ and discharge. The test data of this experimental product are: hydroxyl value of 45.5 and molecular weight of 3329.
Example Embodiment
[0012] Embodiment 3: add the mixture of 500g castor oil and 1.1g powdery sodium methoxide and NaOH in the reaction kettle (mixing in a 1: 1 ratio), be warming up to 130 DEG C, after 1 hour of vacuum dehydration, add 860g of ethylene oxide, After the reaction at 150°C is complete, the temperature is lowered to 80°C for discharging. The test data of this experimental product are: hydroxyl value 60.3, molecular weight 2511.
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