Lithium-base lubricating grease composition with low-pressure oil-separating and low-storage oil-separating performance
A lithium-based grease and composition technology, applied in lubricating compositions, petroleum industry, thickeners, etc., can solve the problems of failure, unsatisfactory oil separation performance, low use temperature, etc., and achieve oil separation performance in storage The effect of excellent, good shear stability, good high temperature performance
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Embodiment 1
[0017] With 560g12-hydroxystearic acid, 4000g mineral base oil (100 ℃ kinematic viscosity is 14.00mm 2 / s) into a 10-liter kettle, heat up to 70-99°C, stir for 20 minutes to dissolve 12-hydroxystearic acid, then dissolve and add 84g of lithium hydroxide, react for 1 hour, heat up and dehydrate to a true solution after the reaction state, add the remaining part of the base oil 5000g, cool, then add the additive diphenylamine 50g, solid filler bentonite 50g, graphite 160g, silicon dioxide 200g, other additives T202 (200g), T405 (200g), T321 (100g), and finally After three-axis roller grinding and homogenization into grease, a lithium-based lubricating grease composition with low pressure oil separation and low storage oil separation performance can be obtained. The performance indexes of the prepared lithium-based grease composition are shown in Table 1.
Embodiment 2
[0019] With 400g12-hydroxystearic acid, 4000g mineral base oil (100 ℃ kinematic viscosity is 14.00mm 2 / s) into a 10-liter kettle, heat up to 70-99°C, stir for 20 minutes to dissolve 12-hydroxystearic acid, then dissolve and add 60g of lithium hydroxide, react for 1 hour, heat up and dehydrate to a true solution after the reaction state, add the remaining part of base oil 5000g, cool, then add additives diphenylamine 50g, solid filler bentonite 160g, silica (A) 200g, other additives T202 (200g), TCP (200g), and finally grind by three-axis roller Homogenizing into grease means to prepare a lithium-based lubricating grease composition with low pressure oil separation and low storage oil separation performance. The performance indexes of the prepared lithium-based grease composition are shown in Table 1.
[0020] Table 1
[0021] Pilot projects
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