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91results about How to "Improve shear stability" patented technology

Multifunctional superstrong extreme pressure antiwear lubricating grease and preparation method thereof

The invention relates to superstrong extreme pressure antiwear lubricating grease and a preparation method thereof; particularly, a densifier is generated by calcium sulfonate with a high base number through a phase inversion reaction, and the lubricating grease is prepared by combining base oil with other functional additives, wherein the base oil is combined by base oil with high viscosity and medium viscosity. The method comprises the following steps: stirring and mixing the composite base oil and the calcium sulfonate in a reaction vessel, heating, adding a phase inversion promoter, glacial acetic acid, and water, heating and reacting at a constant temperature, adding calcium hydrate, aliphatic acid and boric acid after the phase inversion is completed, reacting at a constant temperature, heating and dehydrating, adding an anti-oxidant, refining, transferring the materials into a blending vessel, adding an eutectic rolling additive and an adhesion improver, dispersing and homogenizing the mixture, filtering, and degassing to obtain the finished product. The lubricating grease of the invention has excellent water sprinkling resistance, excellent high and low temperature performance, superstrong extreme pressure antiwear performance, excellent pumping performance, outstanding shearing stability, and antirust performance.
Owner:超美科技(深圳)有限公司

Anti-rust extreme pressure lithium lubricating grease composition and preparation method

The invention relates to an anti-rust extreme pressure lithium lubricating grease composition and a preparation method thereof. The composition is prepared from 5.5%-12.5% of thickening agents, 72.8%-91.3% of base oil, 0.5%-3.8% of extreme pressure anti-wear agents, 0.28%-1.25% of antioxidants and 0.02%-1.05% of anti-rust anti-corrosion agents, wherein the base oil is high-viscosity mineral oil. The preparation method of the composition comprises the steps that one third of the base oil and 12-hydroxy stearin or a mixture of 12-hydroxy stearin and stearic acid are heated to the temperature ranging from 60 DEG C to 80 DEG C, a lithium hydroxide solution is added, the temperature is raised to range from 180 DEG C to 220 DEG C after a reaction is completed, one third of quenching oil is added, the extreme pressure anti-wear agents, the anti-rust anti-corrosion agents and the rest of the base oil are added after cooling is conducted, and the composition is prepared after grounding is conducted. The novel lubricating grease containing the extreme pressure components and the anti-rust anti-corrosion components has the excellent extreme pressure property and anti-corrosion property and can be widely applied to severer environment conditions with a medium or heavy load and water.
Owner:CHINA PETROLEUM & CHEM CORP

Lubricating grease containing modified silica component and preparation method of lubricating grease

The invention relates to lubricating grease containing a modified silica component and a preparation method of the lubricating grease. The excellent properties of silicone grease and lithium lubricating grease are well combined through modified SiO2. With total weight of a composition as benchmark, the lubricating grease provided by the invention comprises the following components: a thickening agent accounting for 10-25% of the total weight and including 12-hydroxystearic acid, stearic acid and the modified SiO2; base oil accounting for 73-88% of the total weight and consisting of synthetic oil and mineral oil; and additives mainly including the following three types: (a) 0.6-1.8% of anti-wear reagent at extreme pressure, (b) 0.32-1.32% of antioxidant, and (c) 0.02-0.04% of antirust preservative. The novel lubricating grease containing modified SiO2 has excellent shear stability and storage stability and is a kind of SiO2-containing lithium lubricating grease in which high and low temperature, colloid stability and water resistance are greatly improved. The lubricating grease is especially suitable for application under harsh environmental conditions of high temperature and heavy load.
Owner:CHINA PETROLEUM & CHEM CORP

Modified SiO2 lubricating grease and preparation method thereof

The invention discloses a modified SiO2 lubricating grease and a preparation method thereof. The modified SiO2 lubricating grease comprises the following components by mass: 8-12% of a thickening agent, 45-65% of base oil, and 3-5% of a modifier. The thickening agent is industrial SiO2, the base oil is NBR silicone oil, dimethicone and PAO-40 oil, and the modifier is silanol. The preparation method includes: putting 45-65% of base oil into a reaction kettle, raising the temperature to 155-160DEG C, adding 3-5% of the modifier, further raising the temperature and fully mixing the materials to make the modifier fully dissolved in the base oil; and when the temperature is raised to 160-165DEG C, adding 8-12% of the thickening agent, stirring the mixture uniformly, and carrying out oil rolling by a three-roller grinding mill, thus obtaining the modified SiO2 lubricating grease. According to the invention, the industrial product SiO2 with small particle size, large specific surface area and controllable surface is adopted as the thickening agent, thus facilitating quick formation of a grid structure and reaching a new equilibrium state. Thus, the obtained SiO2 lubricating grease has good storage stability and shear stability. By using silanol as the modifier, the compatibility of SiO2 particles and the base oil is enhanced.
Owner:WUXI FEITIAN GREASE

Lubricating grease for shear-resistant bearings, and preparation method thereof

The invention relates to a lubricating grease for shear-resistant bearings, and a preparation method thereof. The preparation method comprises the following steps: adding diphenylmethane diisocyanateand a part of base oil into a reaction kettle A according to a ratio of a polyureido group to a lithium base being 1:8 to 1:10, heating the reaction kettle to 50 DEG C, adding two amines molten by a part of the base oil after the diphenylmethane diisocyanate is completely molten, carrying out a reaction, heating the reaction kettle A to a refining temperature of 90 DEG C, keeping the temperature unchanged for 1 h, adding the remaining base oil and all 12-hydroxystearic acid into a reaction kettle B, heating the reaction kettle to 80 DEG C, pouring the obtained mixture into the reaction kettleA after the 12-hydroxystearic acid is completely molten, and dropwise adding an aqueous solution of LiOH into the reaction kettle A to carry out saponification for 0.5 h; adding 0.1% of water after the saponification is finished, and heating the reaction kettle A to 185 DEG C; and keeping the temperature unchanged for 1-2 h, adding an antioxidant, naturally cooling the reaction kettle to 85 DEG C,adding other additives, uniformly stirring above substances, carrying out rolling oil fine filtration, and filling the finished degassed finished product.
Owner:CHINA PETROLEUM & CHEM CORP

Long-acting wire rope hemp core grease

The invention relates to a long-acting wire rope hemp core grease. The long-acting wire rope hemp core grease comprises 13-17wt% of palm wax, 16-19wt% of microcrystalline wax, 15-19wt% of naphthenic high-viscosity oil, 24-28wt% of paraffinic high-viscosity oil, 1.6-4.6wt% of zinc dialkyl dithiophosphate, 1.4-4.4wt% of nonyldiphenylamine, 4.5-8.5wt% of vinylacetic acid, 8.5-12.5wt% of polyisobutylene and 0.1-1wt% of calcium sulfonate. Compared with hemp core greases in the prior art, the long-acting wire rope hemp core grease has the advantages of high dropping point, no flowing in hot weather, fast online solidification after rope immersion, no loss, energy saving, no pollution to environment, large kinematic viscosity data, good adhesiveness, and realization of good fluidity and no flowing of a grease film in the motion and compressed processes. Prominently, the property of traditional hemp core greases (including imported hemp core greases) is changed to become weakly alkaline (the free base value is not greater than 0.15, NaOH%), so oxidation is effectively inhibited, generated free acids are neutralized, SH/T0325 oxidation stability test and SH/T0331 corrosion test are extremely well passed, the safe service life of a wire rope is effectively prolonged, and use environment is purified.
Owner:GUANGZHOU ROSTON PETROCHEM CO LTD

High extreme pressure lithium-based lubricating grease

The invention relates to high extreme pressure lithium-based lubricating grease. The production process comprises the following steps: adding 1/2 of base oil high-viscosity mineral oil, fatty acid, lithium hydroxide and calcium hydroxide according to the stipulated mixture ratio in parts by weight, performing saponification reaction at the temperature of 100 DEG C, then adding the heated oil, namely the remaining 1/2 of the base oil high-viscosity mineral oil, heating to 200 DEG C to the greatest extent to perform high-temperature refining, then cooling to 180 DEG C, further cooling to 110 DEG C, adding an antioxidant, an extreme pressure agent, an oily agent and a tackifier, then performing post-treatment by using a homogenizer or a cyclic shearing machine, filtering and packaging. Tests prove that the grease becomes thin when meeting water, the thinness is far less than that of traditional extreme pressure lithium, the grease is less prone to loss and can provide good anti-rust protection for bearings, when the water content in the grease is 15%, the extreme pressure performance is reduced to a smaller extent and higher than the extreme pressure performance of the traditional extreme pressure lithium grease, the bearings are not worn at all, the production is not affected, and the grease is very suitable for high load, high temperature, high speed and much water working conditions of the bearings.
Owner:青州市东能润滑油脂有限公司
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