Preparation containing organosilicium compound and its use
A technology of organosilicon compounds and mixtures, used in anti-corrosion coatings, transportation and packaging, thin material processing, etc.
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Embodiment 1
[0148] Preparation of Powder 1
[0149] Within 15 minutes with a propeller stirrer and under the condition of 1000Upm in 329.2g saponification degree is 88mol% and 4% solution 100g emulsified in an aqueous solution of 24% by weight polyvinyl alcohol with a viscosity of 4mPas It is then diluted with water to a solids content of 25% by weight. The mixture was sprayed with compressed air at an inlet temperature of 120° C. on a laboratory spray tower with a two-material nozzle and dried. As antisticking agents, 0.6% by weight of calcined silicic acid and 9.4% by weight of commercially available carbonates, both relative to the shaped powder, were added. A free-flowing, well-redispersible white powder in water was obtained in good yields, which itself did not feel sticky when passed between the fingers and thus contained the acrylic acid used in very good encapsulated form. base alkoxysiloxane mixture.
Embodiment 2
[0151] Preparation of Powder 2
[0152] Example 1 was repeated without diluting the resulting mixture with water. The solids content was 37.9% by weight and the Brookfield viscosity measured with a Spindel 3 at 20 rpm and 25° C. was 1590 mPas. Spray drying was performed using a spray pan at an inlet temperature of 150°C. A free-flowing, well-wetting and well-redispersible white powder is obtained in good yields, which disintegrates into primary granules within a short time when agitated with water.
Embodiment 3
[0154] Preparation of Powder 3
[0155] Mix 329.2g degree of saponification similar to embodiment 2 and be 88mol% and 4% solution Aqueous solution of 24% by weight polyvinyl alcohol with a viscosity of 4mPas and 200.0g of 50% by weight of emulsifier-stabilized Emulsion in water, diluted, dried and blended with anti-sticking agent. A free-flowing, well-wetting and well-redispersible white powder in water was obtained in good yields, which itself did not feel sticky when passed between the fingers and thus encapsulated well The form contains the silicone used.
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