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Fixed bed reactor

A fixed bed reactor and reactor technology, which is applied in chemical instruments and methods, pressure vessels used in chemical processes, chemical/physical processes, etc. Reactor heat transfer efficiency and other issues, to achieve the effect of good acid and alkali corrosion resistance, uniform heating, solving material and processing problems

Inactive Publication Date: 2009-09-23
TAIYUAN UNIV OF TECH
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  • Abstract
  • Description
  • Claims
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Problems solved by technology

The existing problems are that the stainless steel material is not resistant to strong acid or strong alkali corrosion; the second is that the stainless steel reactor lining is made of anti-corrosion non-metallic materials, which reduces the heat transfer efficiency of the reactor; Can withstand higher pressure (10Mpa)
[0006] Due to the limitation of high temperature (700-1100°C) and high pressure (6-10Mpa), the existing reaction equipment cannot meet the temperature and pressure of heat introduction (endothermic) reactions such as methane carbon dioxide reforming reaction and coal methanation. requirements

Method used

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  • Fixed bed reactor

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Embodiment approach 1

[0015] Implement the fixed bed reactor of the present invention, including the molding method of the fixed bed reactor, and the processing method for the shell formed by the flanged cylinder and the head, and the material for making the reactor shell adopts 0Cr18Ni9 , cylinder diameter is 370mm, wall thickness is 40mm. Both the head I and the head II adopt the spherical head with the best force and are welded to the cylinder body. The central end of the head I is welded with the reaction gas outlet pipe 4 and connected to the flange. The central end of the head II is welded with a reaction gas inlet pipe 5 and connected to a flange. A flange 3 is arranged on the cylinder body, and a quartz reaction tube 7 with a diameter of 37 mm and a length of 1000 mm is arranged in the center of the housing 18 on the right side of the flange sealing surface 17 in the flange 3, and one end thereof reaches the flange sealing surface 17, And communicate with the inner chamber of the reactor, ...

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Abstract

The invention relates to a fixed bed reactor which is provided with a quartz reaction tube at the central of a right shell of a flange sealing face; one end of the quartz reaction tube to the flange sealing face is communicated with the inner chamber of the reactor and the other end extends outside the shell; the quartz reaction tube is externally sheathed with an electric heater unit; the center of a left shell of the flange sealing face is provided with an air through pipe; the right end of the air through pipe is butted with the left end of the quartz reaction tube and is communicated with the inner chamber of the reactor and the other end extends outside the shell; the shell of the fixed bed reactor is filled with high temperature material so that the temperature of the wall of a reaction high temperature conductive device is reduced below 50 DEG C; the quartz reaction tube is butted with the air through pipe at the flange sealing face so that the inside and outside pressure of the quartz tube is equal during high temperature reaction; the quartz tube is sheathed with the electric heater unit for directly heating reaction gas, thus greatly increasing heat transfer efficiency and saving power source. The fixed bed reactor is suitable for high temperature and high pressure reaction conditions of methane carbon dioxide reforming reaction, and has simple structure and convenient operation.

Description

technical field [0001] The invention relates to a fixed-bed reactor, in particular to a high-temperature and high-pressure fixed-bed reactor in which a heating device is arranged in the center of a shell composed of a flange-connected cylinder body and a head. Background technique [0002] Chemical production and research often involve high-temperature and high-pressure reaction process conditions. For example, methane carbon dioxide reforming reaction is a strong endothermic reaction, which needs to be carried out at high temperature (700-1100°C); research on methane carbon dioxide reforming under pressurized conditions When making synthesis gas, the reaction is usually carried out under the pressure as high as (6Mpa-10Mpa). Another example, the methanation of coal usually takes place at a temperature of 500-900°C and a pressure of 3-6Mpa. The harsh reaction conditions of this type of heat introduction (endothermic) reaction put forward high requirements on the structure an...

Claims

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Application Information

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IPC IPC(8): B01J3/04B01J8/06
Inventor 董跃张丙模王丽萍赵文军张永发
Owner TAIYUAN UNIV OF TECH
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