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Tower of internal thermal coupling distillation tower and control process thereof

A technology of internal thermal coupling and distillation tower, applied in the direction of fractionation, etc., can solve the problems of high cost, complex structure, difficult application and promotion, etc., and achieve the effect of improving operation flexibility

Inactive Publication Date: 2011-07-20
BEIJING UNIV OF CHEM TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although it has a larger heat transfer area than the concentric cylindrical heat transfer structure, its structure is very complicated and expensive, and it is difficult to be applied and popularized in the actual process.

Method used

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  • Tower of internal thermal coupling distillation tower and control process thereof
  • Tower of internal thermal coupling distillation tower and control process thereof
  • Tower of internal thermal coupling distillation tower and control process thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] The connection mode of the tower of the internal thermally coupled distillation tower obtained after the implementation of technical scheme 1 of the present invention is: the feed enters the preprocessor through the pipeline, and enters the feed plate through the pipeline after pretreatment, that is, the first piece of the stripping section Tray; the top of the stripping section is connected to one end of the compressor through a pipeline; the other end of the compressor is connected to the bottom of the rectifying section; the bottom of the rectifying section is connected to one end of the throttle valve; the other end of the throttle valve is connected to the stripping The top of the section is connected; there are three heat exchangers connected between the rectification section and the stripping section, which are the top heat exchanger, the middle heat exchanger and the bottom heat exchanger; one end of the top heat exchanger is connected to the rectification section...

Embodiment 2

[0033] The connection mode of the column device of the internal thermally coupled distillation tower obtained after the implementation of technical scheme 2 of the present invention is: the feed enters the preprocessor through the pipeline, and enters the feed plate through the pipeline after pretreatment, that is, the first piece of the stripping section Tray; the top of the stripping section is connected to one end of the compressor through a pipeline; the other end of the compressor is connected to the bottom of the rectifying section; the bottom of the rectifying section is connected to one end of the throttle valve; the other end of the throttle valve is connected to the stripping The top of the section is connected; there are three heat exchangers connected between the rectification section and the stripping section, which are the top heat exchanger, the middle heat exchanger and the bottom heat exchanger; one end of the top heat exchanger is connected to the rectification...

example 1

[0037] Example 1: Separation of ethylene / ethane binary mixture by using the column device of the internal thermally coupled distillation column obtained after the implementation of the present invention. An ethylene / ethane binary mixture with a feed flow rate of 988.034 kmol / h and a molar composition of 83 / 17 is separated into two streams of 99.5 mol% ethylene and 99.9 mol% ethane. And compared with conventional distillation tower.

[0038] Figure 4 It is a column device of a conventional distillation column for separating ethylene / ethane. The total plate number of the column is 93, the column height is 68.028m, and the column diameter is 2.253m. The feed flow rate is F=988.034 kmol / h, and the feed position is the 58th tray, which is the position shown by 12 in the figure. After the separation, the tower top discharge is ethylene, the liquid phase molar concentration of the product is 99.5mol%, and the flow rate of the top discharge is 824.042kmol / h; the bottom discharge is...

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Abstract

The invention relates to a tower of an internal thermal coupling distillation tower and a control process thereof; the tower realizes the thermal coupling between a rectifying section and a stripping section only by using three external heat exchangers, one external heat exchanger is used for carrying out heat exchange between the top of the rectifying section and the top of the stripping sectionto realize the operation without external reflux of the internal thermal coupling distillation tower. One external heat exchanger is used for carrying out the heat exchange between the bottom of the rectifying section and the bottom of the stripping section, thus realizing the operation without external backheating of the internal thermal coupling distillation tower. One external heat exchanger is used for carrying out exchange between the middle of the rectifying section and the middle of the stripping section, thus realizing the thermal coupling action between the rectifying section and thestripping section. In the invention, the heat exchangers are arranged outside the rectifying section and the stripping section for facilitating the areas of the heat exchangers not to be limited by the distillation process any more, thus ensuring enough heat exchange areas. Due to the heat exchangers arranged at the top of the rectifying section and the bottom of the stripping section, the operation elasticity, dynamic characteristic and controllability of the distillation tower are improved.

Description

technical field [0001] The invention relates to a tower device with an internal heat coupling distillation tower and its control technology. Background technique [0002] The research on internal thermally coupled distillation columns began in the late 1970s, with the main purpose of solving the long-standing problem of high energy consumption in mixture separation operations based on the second law of thermodynamics. Although it has been proved in theory that the thermal coupling between the rectifying section and the stripping section can make the internal thermally coupled distillation column have very high thermodynamic efficiency, for example, the external reflux ratio and the external heat recovery ratio can be zero ( That is, it breaks the limit of the minimum reflux ratio and the minimum heat recovery ratio), but because this thermal coupling effect is difficult to realize in the design of the distillation column, this efficient internal thermal coupling distillation...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D3/14
Inventor 黄克谨陈海胜武国松王芸张星星王韶锋
Owner BEIJING UNIV OF CHEM TECH
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