Multi-nozzle high-voltage electrostatic spinning apparatus added with electric field shielding device

A high-voltage electrospinning and electric field shielding technology, which is applied in the fields of magnetic field/electric field shielding, complete sets of equipment for the production of artificial wires, electrical components, etc., can solve the problems of incomplete superposition or mixing, weakened mechanical properties, and mutual incompatibility, etc., to achieve Good application promotion value, prevent mutual interference, low cost effect

Inactive Publication Date: 2010-03-17
JILIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] High-voltage electrospinning technology is a micro-nano fiber preparation technology that has received extensive attention in recent years. By adjusting the experimental parameters, the size of the fiber can be adjusted arbitrarily from a few nanometers to tens of microns. It is currently the easiest way to prepare nanofiber materials. , cheap method, the resulting fiber membrane has the advantages of high porosity and large surface area, and is widely used in many fields such as ultrafiltration materials and tissue engineering scaffolds. Pay attention to the ultra-fine size and uniformity of nanofibers, but as the fiber diameter decreases, its mechanical properties are significantly weakened, and it is very easy to break. Although carbon nanotubes are used as reinforcing materials, the strength of the material can be improved, but carbon nanotubes The cost is high and it is not suitable for large-scale fiber preparation. However, using multiple nozzles to superimpose and co-spin microfibers and nanofibers at the same time can form a composite fiber membrane with microfibers as the skeleton and nanofibers as the filling. Combine the high strength of microfibers and the high surface area of ​​nanofibers to solve the problem of poor strength of a single nanofiber; at the same time, in the preparation of materials such as tissue engineering, it is necessary to stack multiple fibers together to form a film with multiple functions , which cannot be sol

Method used

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  • Multi-nozzle high-voltage electrostatic spinning apparatus added with electric field shielding device
  • Multi-nozzle high-voltage electrostatic spinning apparatus added with electric field shielding device
  • Multi-nozzle high-voltage electrostatic spinning apparatus added with electric field shielding device

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0031] Example 1:

[0032] Polyacrylonitrile microfiber and nanofiber co-superposed film

[0033] Dissolve 2g polyacrylonitrile (Mw=100,000) in 18g N,N-dimethylformamide to form a 10% mass concentration solution, keep stirring for 24h for later use;

[0034] Dissolve 4g polyacrylonitrile (Mw=100,000) in 16g N,N-dimethylformamide to form a 20% mass concentration solution, keep stirring for 24h for later use;

[0035] Put the above solution into two medical syringes, each with a needle as an electrospinning nozzle, the nozzles are respectively connected to the anode of the high-voltage power supply, the roller (conducting cylinder with aluminum foil) is the receiver, and the ground is the voltage zero point. Install a bakelite insulation board with a hollow in the middle and a thickness of 1cm on the central shaft of the roller, and place the nozzles on both sides of the insulation bakelite respectively. Keep the bakelite insulation board and the nozzle in a fixed state, and adjust the ...

Example Embodiment

[0036] Example 2:

[0037] As shown in Example 1, the insulating board was replaced with a plexiglass board, and the test results were similar;

Example Embodiment

[0038] Example 3:

[0039] As shown in Example 1, the insulating board was replaced with a tetrafluoroplastic board, and the test results were similar;

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Abstract

The invention belongs to the technical field of high-voltage electrostatic spinning, in particular relates to a multi-nozzle high-voltage electrostatic spinning apparatus which simultaneously co-spinsand superimposes the mono-component or multi-component materials with multi-scale micro-/nano-fiber and multi-scale microsphere fiber and is added with an electric field shielding device. The multi-nozzle high-voltage electrostatic spinning apparatus comprises a high-voltage power supply, a feeding device, a plurality of jet devices with nozzles respectively, a collection device and electric field shielding devices added among the plurality of jet devices. An electrospinning product can be one or more of micro-fiber, nano-fiber, nanosphere and microsphere which coexist at the same time. The prepared micro-/nano-fiber film can be used as an ultra-filtration film, a tissue engineering bracket, a drug slow-release material, and the like. The rough surface formed by the micro-/nano-fiber andthe microsphere can also be applied to the fields of the super-hydrophobic material, and the like. The method has the advantages of simple operation, wide application, relatively low cost, and the like, and has favorable application and generalization value.

Description

technical field [0001] The invention belongs to the technical field of high-voltage electrospinning, and in particular relates to a multi-nozzle with multi-scale micro / nano fibers, multi-scale microspheres / fibers and multi-component materials simultaneously co-spun and superimposed with the addition of an electric field shielding device High-voltage electrospinning equipment. Background technique [0002] High-voltage electrospinning technology is a micro-nano fiber preparation technology that has received extensive attention in recent years. By adjusting the experimental parameters, the size of the fiber can be adjusted arbitrarily from a few nanometers to tens of microns. It is currently the easiest way to prepare nanofiber materials. , cheap method, the resulting fiber membrane has the advantages of high porosity and large surface area, and is widely used in many fields such as ultrafiltration materials and tissue engineering scaffolds. Pay attention to the ultra-fine si...

Claims

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Application Information

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IPC IPC(8): D01D5/00D01D13/00H05K9/00
Inventor 杨清彪李耀先张朝群战乃乾宋岩
Owner JILIN UNIV
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