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Method for filtering and separating red mud in sintering process

A technology of filtration separation and sintering method, applied in filtration separation, separation methods, chemical instruments and methods, etc., can solve the problems of high alumina supersaturation, difficulty in filtration of dissolved red mud, and variability of dissolved red mud, etc. The effect of increasing the liquid concentration, eliminating the limitation of the sedimentation capacity of red mud, and improving the dissolution rate of alumina

Inactive Publication Date: 2010-06-16
GUIZHOU BRANCH CHINA ALUMINUM IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the easy denaturation of the red mud dissolved by the sintering method, the high supersaturation of alumina in the eluate, and the low concentration of alumina, the use of a rubber belt filter to filter and separate the red mud usually results in the hardening of the filter cloth, which makes the red mud dissolved Difficult to filter, causing production disruption

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] The DU type rubber belt filter is used to feed the stripping slurry into the stripping slurry. After the solid-liquid separation of the stripping slurry, the red mud is washed with washing liquid, and the washing liquid is washed once with hot water at 100°C. The filtrate enters the corresponding filtrate tank. The filtrate in the filtering area of ​​the filter is crude liquid, which enters the crude liquid tank through the chute; the filtrate in the washing area of ​​the filter is the washing liquid, which enters the washing liquid tank; the filter cake is discharged outside. During the red mud filtration process, the filter cloth of the filter machine is regenerated by water washing and lye soaking; the red mud filtration and washing area is kept warm to keep the operating environment temperature of the rubber belt filter at 95°C.

Embodiment 2

[0016] Send the stripping slurry to the DU rubber belt filter for filtration. After the solid-liquid separation of the stripping slurry, the red mud is washed with washing liquid. The washing liquid is washed 4 times with hot water at 60°C; the filtrate enters the corresponding filtrate groove. The filtrate in the filtering area of ​​the filter is crude liquid, which enters the crude liquid tank through the chute; the filtrate in the washing area of ​​the filter is the washing liquid, which enters the washing liquid tank; the filter cake is discharged outside. During the red mud filtration process, the filter cloth of the filter machine is regenerated by water washing and lye soaking; the red mud filtration and washing area is kept warm, and the operating environment temperature of the rubber belt filter is kept at 60°C.

Embodiment 3

[0018] Send the dissolved slurry to a DU rubber belt filter for filtration. After the solid-liquid separation of the dissolved slurry, the red mud is washed with washing liquid. The washing liquid is washed twice with hot water at 90°C; the filtrate enters the corresponding filtrate groove. The filtrate in the filtering area of ​​the filter is crude liquid, which enters the crude liquid tank through the chute; the filtrate in the washing area of ​​the filter is the washing liquid, which enters the washing liquid tank; the filter cake is discharged outside. During the red mud filtration process, the filter cloth of the filter machine is regenerated by water washing and lye soaking; the red mud filtration and washing area is kept warm, and the operating environment temperature of the rubber belt filter is kept at 95°C.

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Abstract

The invention discloses a method for filtering and separating red mud in a sintering process, and relates to a method for separating and washing red mud dissolved out from alumina production by the sintering process. A rubber belt filter is adopted to filter the red mud dissolved out in the sintering process; and the method is characterized in that: in the filtering and separating process, after the dissolved-out red mud enters the rubber belt filter, the red mud is subjected to solid-liquid separation first, and filter liquor which is crude solution is subjected to silicon removal; and the red mud separated from the crude solution continuously moves ahead on the filter along with belt filter cloth, and cleaning solution is injected to the red mud after the separation for washing separation. The method can effectively realize quick separation of the red mud dissolved out in the sintering process, reduce secondary reaction loss in a process of dissolving out and separating clinker, and improve the dissolution rate of alumina. Meanwhile, the water quantity for washing the red mud is reduced, the limitation to the sedimentation capacity of the red mud is eliminated, and the concentration of the crude solution after the red mud is separated can be greatly improved, so the production efficiency of the alumina by the sintering process is improved.

Description

technical field [0001] The invention discloses a method for filtering and separating sintering process red mud, and relates to a separation and washing method for sintering process alumina to produce dissolved red mud. technical background [0002] In the process of sintering alumina production, the separation of red mud from clinker dissolution is a key link. At present, most manufacturers adopt the sedimentation tank separation process. Since the settling tank relies on the principle of gravity separation to achieve liquid-solid separation, it is difficult to achieve effective sedimentation separation when the particle size of the solid phase is small, or the specific gravity difference between solid and liquid is small. When crude liquid Al 2 o 3 When the concentration is greater than 130g / l, the sedimentation rate of the red mud in the dissolution slurry will be very slow, and the sedimentation separation cannot achieve effective solid-liquid separation. In addition,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D33/60C01F7/02
Inventor 于斌张占明张立强李文化杨志民唐海红娄世斌张攀峰李云忠范喜威
Owner GUIZHOU BRANCH CHINA ALUMINUM IND
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