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Preparation method of sodium nitrite standard sample for food safety rapid detecting box

A technology of sodium nitrite and food safety, which is applied in the preparation of test samples, material analysis by observing the influence of chemical indicators, and analysis by making materials undergo chemical reactions, etc. methods, large detection errors, etc., to achieve the effect of easy storage and avoid detection errors

Inactive Publication Date: 2014-04-16
贵州省理化测试分析研究中心
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The currently used food safety rapid detection box uses a colorimetric card for standard calibration. The detection of formaldehyde, sulfur dioxide, and nitrite in the rapid detection box is a colorimetric reaction. All colorimetric reactions must follow the temperature, pH, and the amount of color developer. The four elements of reaction time and reaction time, in which the reaction temperature, the amount of developer and the reaction time are related to the operator; while the color comparison card is a standard color comparison card, the operator cannot control it, which will cause a large detection error
[0004] After retrieval, in the Chinese patent database, applications involving food safety testing equipment include No. 03240360.7 "Multifunctional Food Toxic Chemical Contaminant Residue Detector", No. 200410013417.8 "Multi-channel Handheld Food Safety Detector", No. Safety Multi-item Rapid Detector", No. 200720112697.7 "A Quick Detector for Food Safety" and No. 200910079872.0 "A Multifunctional Expanded Food Safety Rapid Detector", etc. These patented technologies still use traditional color cards, and there is no Use operator-controlled detection methods

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] Example 1 Preparation of sodium nitrite standard sample: first dry sodium chloride with a purity of ≥99.5% and constant weight, then dry sodium nitrite with a purity of ≥99.9% and constant weight; then take 50.0 g of sodium chloride and 0.05 G sodium nitrite is mixed and ground evenly, the fineness is less than or equal to 400 mesh, and the content is 1000mg / kg; it is packed in white capsules, each 0.100g, to obtain the standard sample of sodium nitrite.

Embodiment 2

[0017] Example 2 Take 3.5g of ham sausage sample (the appropriate weighing amount is calculated according to the limit standard) and dissolve it in 10mL of water, shake it fully, let it stand still, and wait for the test. Take out the nitrite calibration sample, open it, and put it into a dry, clean small beaker; add 10mL of distilled water to the small beaker to dissolve and shake well. Take 1 mL of the above solution, add 9 mL of water and shake well to make a calibration solution. Take 1mL of calibration solution and sample supernatant respectively, add 9mL of distilled water respectively, and shake well. Then take 1mL respectively, add it to the detection tube, cover it, shake the reagent to dissolve, and compare the color of the sample with the calibration sample after 10 minutes. If the color of the sample is lighter than the calibration sample, then the sample is qualified; if the color of the sample is darker than the calibration sample, then the sample needs to be fu...

Embodiment 3

[0018] Example 3 Take 2g of canned meat sample (the appropriate weighing amount is calculated according to the limit standard) and dissolve it in 10mL of water, shake fully, stand still, and wait for the test. Take out the nitrite calibration sample capsule, open it, and put it into a dry, clean small beaker; add 10mL of distilled water to the small beaker to dissolve and shake well. Take 1 mL of the above solution, add 9 mL of water and shake well to make a calibration solution. Take 1mL of calibration solution and sample supernatant respectively, add 9mL of distilled water respectively, and shake well. Then take 1mL respectively, add it to the detection tube, cover it, shake the reagent to dissolve, and compare the color of the sample with the calibration sample after 10 minutes. If the color of the sample is lighter than the calibration sample, then the sample is qualified; if the color of the sample is darker than the calibration sample, then the sample needs to be furthe...

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PUM

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Abstract

The invention discloses a preparation method of a sodium nitrite standard sample for a food safety rapid detecting box. The method comprises the following steps: (1) drying sodium chloride, keeping the weight constant; (2) drying sodium nitrite, keeping the weight constant; (3) mixing sodium chloride and sodium nitrite, grinding uniformly; and (4) subpackaging with a white capsule to obtain a sodium nitrite standard sample. The sodium nitrite standard sample is a solid sample; when in use, a defined amount of distilled water is used to dissolve the solid standard sample, thus the standard sample is easy and convenient to use; the inspector performs all the operations of the calibration sample and samples and the four factors, namely control temperature, pH value, dosage of color reagent and reaction time can be consistent, thus the detection error of the traditional method can be avoided; the solid calibration sample is filled in a tube, thus the cost is low and the sample is convenient to carry and easy to store and can not be volatilized; and the solid calibration sample is used for color comparison, thus the inspector can intuitively judge whether a detected sample exceeds a standard or not without checking the standard. The method is suitable for the common food safety rapid detecting box.

Description

technical field [0001] The present invention is related to the detection of objects by optical means, and more specifically, to the detection of food. Background technique [0002] Since 2004, my country has widely promoted food safety rapid inspection technology. Through rapid inspection of products, inspectors can conduct real-time inspections of food safety such as grain, vegetables, fruits, meat, and aquatic products in communities, supermarkets, farmers markets, restaurants, etc. Monitoring and spot checks at any time. Using the rapid detection technology, it can be detected whether there is Sudan red in chili sauce in 10 minutes, and whether steamed buns contain carcinogenic substances such as white block, formaldehyde, sulfur dioxide and other prohibited chemical components in 13 minutes. In addition, vegetable pesticide residues, pickled The nitrite content of food can also be quickly detected. [0003] The currently used food safety rapid detection box uses a color...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N1/38G01N21/78
Inventor 谢锋谭红陆洋舒海霞杨鸿波张清海李荣华宋光林罗艳何锦林周慧文锡梅
Owner 贵州省理化测试分析研究中心