Preparation method of sodium nitrite standard sample for food safety rapid detecting box
A technology of sodium nitrite and food safety, which is applied in the preparation of test samples, material analysis by observing the influence of chemical indicators, and analysis by making materials undergo chemical reactions, etc. methods, large detection errors, etc., to achieve the effect of easy storage and avoid detection errors
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Embodiment 1
[0016] Example 1 Preparation of sodium nitrite standard sample: first dry sodium chloride with a purity of ≥99.5% and constant weight, then dry sodium nitrite with a purity of ≥99.9% and constant weight; then take 50.0 g of sodium chloride and 0.05 G sodium nitrite is mixed and ground evenly, the fineness is less than or equal to 400 mesh, and the content is 1000mg / kg; it is packed in white capsules, each 0.100g, to obtain the standard sample of sodium nitrite.
Embodiment 2
[0017] Example 2 Take 3.5g of ham sausage sample (the appropriate weighing amount is calculated according to the limit standard) and dissolve it in 10mL of water, shake it fully, let it stand still, and wait for the test. Take out the nitrite calibration sample, open it, and put it into a dry, clean small beaker; add 10mL of distilled water to the small beaker to dissolve and shake well. Take 1 mL of the above solution, add 9 mL of water and shake well to make a calibration solution. Take 1mL of calibration solution and sample supernatant respectively, add 9mL of distilled water respectively, and shake well. Then take 1mL respectively, add it to the detection tube, cover it, shake the reagent to dissolve, and compare the color of the sample with the calibration sample after 10 minutes. If the color of the sample is lighter than the calibration sample, then the sample is qualified; if the color of the sample is darker than the calibration sample, then the sample needs to be fu...
Embodiment 3
[0018] Example 3 Take 2g of canned meat sample (the appropriate weighing amount is calculated according to the limit standard) and dissolve it in 10mL of water, shake fully, stand still, and wait for the test. Take out the nitrite calibration sample capsule, open it, and put it into a dry, clean small beaker; add 10mL of distilled water to the small beaker to dissolve and shake well. Take 1 mL of the above solution, add 9 mL of water and shake well to make a calibration solution. Take 1mL of calibration solution and sample supernatant respectively, add 9mL of distilled water respectively, and shake well. Then take 1mL respectively, add it to the detection tube, cover it, shake the reagent to dissolve, and compare the color of the sample with the calibration sample after 10 minutes. If the color of the sample is lighter than the calibration sample, then the sample is qualified; if the color of the sample is darker than the calibration sample, then the sample needs to be furthe...
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