Processing method of shale oil
A processing method and technology for shale oil, which are applied in the petroleum industry, refining hydrocarbon oil, and multi-stage series refining process treatment, etc., can solve the problems of single product, complex process, high hydrogen consumption and operating cost
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Embodiment 1
[0014] Example 1: Take 40kg of Jilin Huadian shale oil and 40kg of N-methylpyrrolidone extractant, put them into an extraction and separation apparatus and mix them, heat up to 25°C, and start stirring to make the shale oil and N-methylpyrrolidone extractant fully Mixed contacts. Stirring was stopped after 30 minutes, the extract phase and the raffinate phase were allowed to stand for 30 minutes to separate layers, and the extract phase was released from the discharge port to separate the extract phase from the raffinate phase. The extract phase and the raffinate phase are distilled separately to obtain extract oil, raffinate oil and N-methylpyrrolidone extractant respectively, and the obtained extractant is recovered.
[0015] The extracted oil was separated by distillation under reduced pressure to obtain 8% light components and 92% heavy components by weight respectively. It has been determined that the index of the heavy component can meet the standard of heavy traffic as...
Embodiment 2
[0016] Example 2: Take 40 kg of Fushun shale oil and 10 kg of furfural extractant, put them into an extraction separator and mix them, raise the temperature to 60° C., start stirring, so that the shale oil and furfural extractant are fully mixed and contacted. After 60 minutes, the stirring was stopped, and the extract phase and the raffinate phase were left to stand for 60 minutes, and the extract phase was released from the discharge port to separate the extract phase and the raffinate phase. The extraction phase and raffinate phase are distilled separately to obtain extracted oil, raffinate oil and furfural extractant respectively, and the obtained extractant is recovered.
[0017] The extracted oil was separated by distillation under reduced pressure to obtain 6% light components and 94% heavy components by weight respectively. It has been determined that the index of the heavy component can meet the standard of heavy traffic asphalt (GB / T 15180-2000) AH-70, and can be mad...
Embodiment 3
[0018] Example 3: Take 60 kg of Jilin Huadian shale oil and 10 kg of N-methylpyrrolidone extractant, put them into an extraction and separation apparatus for mixing, heat up to 85° C., and start stirring to make the shale oil and N-methylpyrrolidone extractant fully Mixed contacts. Stirring was stopped after 120 minutes, the extract phase and the raffinate phase were allowed to stand for 120 minutes to separate layers, and the extract phase was released from the discharge port to separate the extract phase and the raffinate phase. The extract phase and the raffinate phase are distilled separately to obtain extract oil, raffinate oil and N-methylpyrrolidone extractant respectively, and the obtained extractant is recovered.
[0019] The extracted oil was separated by vacuum distillation to obtain 5% light components and 95% heavy components by weight respectively. It has been determined that the heavy component is close to the 60# road petroleum asphalt index (SH / T 0522-2000), ...
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