Method for extracting lipid components
A technology for lipids and extraction tanks, which is applied in chemical instruments and methods, fat production, and recovery of fatty substances. It can solve problems such as high equipment requirements, flammability and explosion, and limited production scale, and achieve stable chemical properties and extraction efficiency. High, good product quality effect
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Embodiment 1
[0018] Take peanuts with an oil content of 40% by weight, go through impurity removal, shelling, drying, and embryo pressing (the temperature of peanuts should be kept ≤50°C during the process), and then put the embryo flakes into the extraction tank, and vacuumize to below 0.01MPa Finally, add liquefied perfluoropropane that is 1.5 times the weight of the raw material at an operating temperature of 30°C (the operating pressure is the corresponding vapor pressure), and after 60 minutes each time and a total of 3 extractions, a mixture of oil and solvent is obtained; oil and solvent The mixture is decompressed and gasified. After the gauge pressure reaches 0MPa, it is vacuumized and precipitated. When the gauge pressure is -0.09MPa and the temperature is 40~50℃, it is maintained for 30 minutes to obtain the precipitated peanut crude oil, which contains residual solvent ≤ 30mg / kg, impurity ≤0.3%.
[0019] The defatted peanut meal containing solvent is decompressed and gasified,...
Embodiment 2
[0021] Take soybeans with an oil content of 20% by weight, remove impurities, peel, dry, crush, soften, and press embryos (the temperature of soybeans should be kept ≤70°C during the process), and then put the embryo flakes into the extraction tank and vacuumize to 0.01 When it is below MPa, add liquefied perfluorobutane twice the weight of raw materials, operate at 60°C (operating pressure is the corresponding vapor pressure), and extract oil and solvent mixture for 30 minutes each time for a total of 3 times; The mixture of oil and solvent is gasified under reduced pressure, and the gauge pressure reaches 0MPa, and then vacuumizes for precipitation. When the gauge pressure is -0.09MPa and the temperature is 50~60℃, keep for 50 minutes to obtain the crude soybean oil containing residual solvent. ≤50mg / kg, impurity ≤0.3%.
[0022] The solvent-containing defatted soybean meal is decompressed and gasified, and the gauge pressure reaches 0MPa, and then vacuumized for precipitatio...
Embodiment 3
[0024]Take hemp seeds with an oil content of 28% by weight, after screening to remove organic and inorganic impurities and magnetic separation to remove metal impurities, dry them with hot air at a temperature of 40~50°C until the water content drops to ≤8% by weight, and use shelling Machine crushing (keep the temperature of the hemp seeds ≤ 50°C during the crushing process), and then screen the crushed hemp seeds with a sieve, the hemp seeds pass through the sieve, and the shells are blocked by the sieve to obtain shelled hemp Seed kernels; use the embryo pressing machine to press the hemp seed kernels into embryo flakes; put the embryo flakes into the extraction tank, vacuumize to below 0.01MPa, add liquefied perfluorobutane twice the weight of raw materials, and operate at 40 ℃ (the operating pressure is the corresponding vapor pressure), after 20 minutes each time, a total of 4 extractions, the oil and solvent mixture is obtained; the oil and solvent mixture is gasified un...
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