Extraction method of raw total saponins from fresh dioscorea plants
A technology of total saponins and Dioscorea, applied in the field of extraction of crude total saponins, can solve the problems of sufficient solvent contact, affecting the extraction rate and extraction time of the target extract, and achieve the effect of improving the extraction rate
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Embodiment 1
[0019] A method for extracting crude total saponins from fresh yam plants comprises the following steps.
[0020] (1) Crush 100 g of the rhizome of fresh yams into granules, then store them for natural fermentation, and use them as raw materials. The fermentation time is 12 hours.
[0021] (2) Put the fermented raw material into the container, irradiate it with microwave for 40 seconds, and the temperature of the raw material rises to 60°C.
[0022] (3) Further pulverize the raw materials after microwave irradiation, and pulverize them into particles with a size of 40-100 mesh.
[0023] (4) Soak the particles obtained in step 3 in a 65% ethanol solution for 1 minute, and then filter out the mixed solution.
[0024] (5) After the remaining filter residue was irradiated by microwave for 30 seconds, it was soaked again in 65% ethanol solution for 1 minute, and then the mixed solution was filtered out.
[0025] (6) Repeat the process of step 5 for 3 times.
[0026] (7) After c...
Embodiment 2
[0028] A method for extracting crude total saponins from fresh yam plants comprises the following steps.
[0029] (1) Cut 150g of fresh yam rhizomes into flakes, store them for natural fermentation, and use them as raw materials. The fermentation time is 24 hours.
[0030] (2) Dehydrate the fermented raw materials for a while, put them in a container, and irradiate them with microwaves for 90 seconds, and the temperature of the raw materials rises to 90°C.
[0031] (3) The raw material after microwave irradiation is further pulverized into particles with a size of 60-120 mesh.
[0032] (4) Soak the particles obtained in step 3 in a 95% ethanol solution for 3 minutes, and then filter out the mixed solution.
[0033] (5) After the remaining filter residue was irradiated by microwave for 70 seconds, it was soaked again in 85% ethanol solution for 3 minutes, and then the mixed solution was filtered out.
[0034] (6) Repeat the process of step 5 for 3 times.
[0035] (7) After ...
Embodiment 3
[0037] A method for extracting crude total saponins from fresh yam plants comprises the following steps.
[0038] (1) Cut 300 g of fresh yam rhizomes into flakes or crush them into granules, and then store them for natural fermentation as raw materials. The fermentation time was 36 hours.
[0039] (2) Put the fermented raw material into a container, and irradiate it with microwaves for 150 seconds. When the temperature of the raw material rises to 85°C, stop the microwave irradiation.
[0040] (3) The raw material after microwave irradiation is further pulverized into particles with a size of 140 mesh.
[0041] (4) Soak the particles obtained in step 3 in a 90% methanol solution for 5 minutes, and then filter out the mixed solution.
[0042] (5) After the remaining filter residue was irradiated by microwave for 80 seconds, it was soaked again in 75% methanol solution for 5 minutes, and then the mixed solution was filtered out.
[0043] (6) Repeat the process of step 5 for 4...
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