Cooking-resistant polyvinylidene chloride coating film and preparation method thereof
A technology of polyvinylidene chloride and its manufacturing method, which is applied in the direction of chemical instruments and methods, devices for coating liquid on the surface, coatings, etc., and can solve the problems of opaque packaging, short shelf life, and no high-temperature disinfection and sterilization
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Embodiment 1
[0031] Substrate: Biaxially oriented polypropylene (BOPP), 19 μm thick.
[0032] Primer: commercially available polyurethane adhesive
[0033] Polyvinylidene chloride emulsion: commercially available polyvinylidene chloride emulsion
[0034] Demineralized water: homemade 30kg
[0035] Slip agent: commercially available palm wax slip agent 10kg
[0036] Anti-blocking agent: commercially available silica anti-blocking agent 1kg
[0037] Add 50 kg of 50% polyvinylidene chloride emulsion into a 100L reactor, start the reactor and stir at a stirring speed of 120 rpm, slowly raise the temperature, and control the temperature at 50°C. Accurately weigh 250 grams of tetraethylenepentamine, dissolve it in 200ml of deionized water, place it in a 500ml dropper, wait for the temperature of the reaction kettle to become constant, start to add dropwise, the drop rate is 8.6g / min, and keep a constant temperature during the dropwise addition process . After the dropwise addition, the stir...
Embodiment 2
[0044] Substrate: biaxially oriented polyester (BOPET), thickness 12 μm.
[0045] Primer: commercially available polyurethane adhesive
[0046] Polyvinylidene Chloride Emulsion:: Commercially Available Polyvinylidene Chloride Emulsion
[0047] Demineralized water: homemade 25kg
[0048] Slip agent: commercially available palm wax slip agent 9kg
[0049] Anti-blocking agent: commercially available silica anti-blocking agent 1kg
[0050] Add 40 kg of 50% polyvinylidene chloride emulsion into a 100L reactor, start the reactor and stir at a stirring speed of 100 rpm, slowly raise the temperature, and control the temperature at 45°C. Accurately weigh 200 grams of tetraethylenepentamine, dissolve it in 300ml of deionized water, place it in a 1000ml dropper, wait until the temperature of the reaction kettle tends to be constant, start to add dropwise, the drop rate is 9.5g / min, and keep a constant temperature during the dropwise addition process . After the dropwise addition, th...
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