Metastable beta-type Ti-Mo-Si system biomedical alloy and preparation method thereof

A ti-mo-si, biomedical technology, applied in the field of titanium alloys, can solve the problems of high cost, less research and application, etc., and achieve the effect of low production cost, low price, and reduced research and development and production costs

Inactive Publication Date: 2012-05-09
GUANGXI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] At present, there are few researches and applications on the relatively cheap but biocompatible silicon element as an alloying element for medical titanium alloys.
The cost of new biomedical titanium alloy is very high, and it will be industrialized and popularized in the future

Method used

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  • Metastable beta-type Ti-Mo-Si system biomedical alloy and preparation method thereof
  • Metastable beta-type Ti-Mo-Si system biomedical alloy and preparation method thereof
  • Metastable beta-type Ti-Mo-Si system biomedical alloy and preparation method thereof

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Experimental program
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Effect test

Embodiment 1

[0033] 1. Raw material formula: raw material components and weight percentages are: titanium sponge 90.00%, molybdenum 10.00%; the purity of titanium sponge and molybdenum are both above 99%.

[0034] 2. Preparation method:

[0035] The specific steps for preparing metastable β-type Ti-Mo-Si series biomedical alloys are as follows:

[0036] (1) raw material is weighed, according to the percentage by weight of each raw material component, take sponge titanium, molybdenum respectively;

[0037] (2) Raw materials are mixed, and the weighed raw materials are mixed evenly by means of stirring and mixing;

[0038] (3) Raw material smelting, put the uniformly mixed raw material into the crucible in the non-consumable vacuum electric arc furnace, and then vacuumize, the vacuum degree is 1.0×10 -2 ~1.0×10 -3 Pa; then pass in an argon gas of standard atmospheric pressure for gas washing; repeat vacuuming and gas washing for 2 times; finally carry out repeated melting under the protec...

Embodiment 2

[0043] 1. Raw material formula: raw material components and weight percentages are: titanium sponge 89.50%, molybdenum 10.00% and silicon 0.50%; the purity of titanium sponge, molybdenum and silicon are all above 99%.

[0044] 2. Preparation method:

[0045] The specific steps for preparing metastable β-type Ti-Mo-Si series biomedical alloys are as follows:

[0046] (1) raw material is weighed, according to the percentage by weight of each raw material component, take sponge titanium, molybdenum respectively;

[0047] (2) Raw materials are mixed, and the weighed raw materials are mixed evenly by means of stirring and mixing;

[0048] (3) Raw material smelting, put the uniformly mixed raw material into the crucible in the non-consumable vacuum electric arc furnace, and then vacuumize, the vacuum degree is 1.0×10 -2 ~1.0×10 -3Pa; then pass in an argon gas of standard atmospheric pressure for gas washing; repeat vacuuming and gas washing for 3 times; finally carry out repeated...

Embodiment 3

[0053] 1. Raw material formula: raw material components and weight percentages are: titanium sponge 88.75%, molybdenum 10.00% and silicon 1.25%; the purity of titanium sponge, molybdenum and silicon are all above 99%.

[0054] 2. Preparation method:

[0055] The specific steps for preparing metastable β-type Ti-Mo-Si series biomedical alloys are as follows:

[0056] (1) raw material is weighed, according to the percentage by weight of each raw material component, take sponge titanium, molybdenum respectively;

[0057] (2) Raw materials are mixed, and the weighed raw materials are mixed evenly by means of stirring and mixing;

[0058] (3) Raw material smelting, put the uniformly mixed raw material into the crucible in the non-consumable vacuum electric arc furnace, and then vacuumize, the vacuum degree is 1.0×10 -2 ~1.0×10 -3 Pa; then pass in an argon gas of standard atmospheric pressure for gas washing; repeat vacuuming and gas washing for 3 times; finally carry out repeate...

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Abstract

The invention discloses a metastable beta-type Ti-Mo-Si system biomedical alloy and a preparation method thereof. The metastable beta-type Ti-Mo-Si system biomedical alloy comprises the following raw material components in percentage by weight: 88.00-90.00 percent of sponge titanium, 0.00-2.00 percent of silicon and 9.5-10.50 percent of molybdenum. The preparation method comprises the following steps of: firstly, respectively weighing raw material according to the weight percentage of the raw material components; secondly, uniformly mixing the raw materials and melting the raw materials by using non-consumable arc; and finally, cooling to obtain an alloy cast ingot with a uniform structure. According to the metastable beta-type Ti-Mo-Si system biomedical alloy and the preparation method thereof disclosed by the invention, the non-poisonous molybdenum and low-price silicon are added to improve the phase composition and the mechanical property of a titanium alloy, so that the mechanical property of the alloy is better matched with that of natural bone of a human body. The low-price silicon is used as one of alloying elements, so that the production cost of the alloy is effectively reduced.

Description

technical field [0001] The invention belongs to the technical field of titanium alloys, in particular to metastable β-type biomedical titanium alloys. Background technique [0002] Biomedical materials include materials that can be medically implanted into organisms or combined with biological tissues. Biomaterials are used to treat or replace original tissues and organs in biological organisms, and to correct and improve their functions. At present, biomedical metal materials are widely used as surgical implant materials. They have high strength, good toughness, bending fatigue resistance and good processing and forming properties, and have excellent properties that other types of medical materials cannot replace. As biomedical materials, metal materials must meet strict biological requirements: (1) good tissue compatibility, non-toxicity, no distortion, no allergic reaction, no interference with the body's immunity, no damage to adjacent tissues, etc.; (2) physical and che...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C14/00C22C1/02
Inventor 湛永钟李春流
Owner GUANGXI UNIV
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