Freeze-dried powder composition containing Bifidobacterium longum cell lysate and preparation method and application thereof
A technology of Bifidobacterium longum and lysate, which is used in skin care preparations, pharmaceutical formulations, cosmetic preparations, etc., and can solve the problem of preventing aging skin and the combination of Bifidobacterium longum lysate and chicken embryo essence. And other issues
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Embodiment 1
[0062] Example 1 Preparation of Bifidobacterium longum lysate freeze-dried powder
[0063] Mix and dissolve the freeze-dried powder of Bifidobacterium longum and phosphate buffer according to the mass volume ratio (kg / L) 1:5.0, and then use ultrasonic waves to break the cell wall of Bifidobacterium longum. The ultrasonic program is: ultrasonic 3s, interval 3s, ultrasonic 20 cycles. Follow this procedure for 3 more ultrasounds. After sonication, centrifuge at 6000rpm for 20min. Add trehalose to the supernatant after centrifugation according to the mass volume ratio (kg / L) trehalose: solution = 1:3.0, freeze-dry at -80°C for 18 hours to obtain freeze-dried powder of Bifidobacterium longum.
Embodiment 2
[0064] Example 2 Preparation of Lysate of Bifidobacterium longum and Chicken Embryo Essence Composition Freeze-dried Powder
[0065] Mix and dissolve the freeze-dried powder of Bifidobacterium longum and phosphate buffer according to the mass volume ratio (kg / L) 1:5.0, and then use ultrasonic waves to break the cell wall of Bifidobacterium longum. The ultrasonic program is: ultrasonic 3s, interval 3s, ultrasonic 20 cycles. Follow this procedure for 3 more ultrasounds. After sonication, centrifuge at 6000rpm for 20min. Mix the centrifuged supernatant with the chicken embryo essence at a volume ratio of 1.5:1, and add trehalose to the mixture at a mass-volume ratio (kg / L) of trehalose:mixed solution=1:3.0, Freeze-dry at 80°C for 18 hours to obtain a freeze-dried powder of the composition.
[0066] The following is an in vitro test
Embodiment 3
[0067] Example 3 Antioxidant (free radical scavenging) effect of Bifidobacterium longum lysate and chicken embryo essence composition
[0068] Free radicals are one of the main factors leading to skin aging. Antioxidant substances can combine with or replace free radicals, which reduces the number of [DPPH·] free radicals, and the color of the solution becomes lighter, which is manifested as light absorption at 515 nm The value keeps decreasing until it reaches a stable value. Therefore, the antioxidant or free radical scavenging ability can be calculated (judged) by measuring the ability of antioxidant substances to capture [scavenge] free radicals at 515 nm. It is used for anti-oxidation, anti-aging and whitening effects on functional cosmetic raw materials. [DPPH·] (diphenylpicrylhydrazyl radical) is a relatively stable N-centered radical. [DPPH·]methanol solution is purple, and has the maximum light absorption at 515 nm wavelength, and the depth of the color has a line...
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