Cuprous ion selective electrode and cuprous ion measuring method thereof
A cuprous ion and electrode selection technology, which is used in the field of chemical analysis to achieve the effect of meeting application needs
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Embodiment 1
[0037] 1. Electrode preparation
[0038] Cuprous sulfide powder and β-Ag 2 S-type silver sulfide powder is placed in a mold with a mass ratio of 40:60 for tableting to form a solid sheet. then press figure 1 structure, assembled into electrodes.
[0039] 2. Standard curve preparation
[0040] Cu will be prepared separately in five 100mL volumetric flasks + Concentration is 10 -2 mol / L, 10 -3 mol / L, 10 -4 mol / L, 10 -5 mol / L, 10 -6 mol / L standard solution, 10mL of 2mol / L potassium chloride solution as ionic strength regulator. Pour the above five standard solutions into clean and dry beakers respectively, and put in a stirring bar. The prepared cuprous ion selective electrode was inserted into the Cu + Place the beaker of the standard solution on a magnetic stirrer and stir steadily for 2 minutes, then let it stand for 1 minute, and read the potential value E after the potential is stable. The measurement is carried out in order from lean to rich. ΔφM and K are obta...
Embodiment 2
[0047] 1. Electrode preparation
[0048] Cuprous sulfide powder and β-Ag 2 S-type silver sulfide powder is placed in a mold with a mass ratio of 60:40 for tableting to form a solid sheet. then press figure 1 structure, assembled into electrodes.
[0049] 2. Standard curve preparation
[0050] Cu will be prepared separately in five 100mL volumetric flasks + Concentration is 10 -2 mol / L, 10 -3 mol / L, 10 -4 mol / L, 10 -5 mol / L, 10 -6 mol / L standard solution, 10mL of 2mol / L potassium chloride solution as ionic strength regulator. Pour the above five standard solutions into clean and dry beakers respectively, and put in a stirring bar. The prepared cuprous ion selective electrode was inserted into the Cu + Place the beaker of the standard solution on a magnetic stirrer and stir steadily for 2 minutes, then let it stand for 1 minute, and read the potential value E after the potential is stable. The measurement is carried out in order from lean to rich. ΔφM and K are obta...
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