Ganchang preparation quality detection method
A Ganchang and preparation technology, applied in the field of medicine, can solve the problems of inaccurate quality inspection of Ganchang capsule preparations, and the quality standard needs to be improved, and achieve the effect of quality control and quality safety.
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[0482] Embodiment 1: quality detection method
[0483] Identification:
[0484] A. Identification of safflower:
[0485] Take 4g of Ganchang Capsules, add 15ml of acetone with a volume percentage of 80%, seal it tightly, shake it for 20 minutes, let it stand still, absorb the supernatant, and use it as the test solution; take another 1g of safflower reference medicinal material, and prepare the reference medicinal material solution in the same way According to the thin-layer chromatography (Appendix VIB) test, draw 10 μl of each of the above two solutions, and place them on the same silica gel G thin-layer plate with sodium carboxymethylcellulose as the binder, and the volume-to-number ratio is 8: 2: 2 ethyl acetate-formic acid-water as the developing agent, develop, take out, and dry; in the chromatogram of the test product, on the position corresponding to the chromatogram of the control medicinal material, spots of the same color appear;
[0486] B. Identification of wave...
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