Method for in-situ preparing nano-silver compound bactericide
A compound bactericide, in-situ preparation technology, applied in the field of material chemistry, can solve the problems of unsatisfactory bactericidal effect, inability to bond firmly, complicated preparation process, etc., achieve superior environmental friendliness and human safety, good physical and chemical properties, The effect of improving the bactericidal performance
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Embodiment 1
[0014] Measure 20mL0.1mol / L CaCl 2 Aqueous solution, 20mL0.06mol / L KH 2 PO 4 Add 0.02 g of polyethylene glycol to the aqueous solution, place the two solutions on both sides of the casing, let stand for 10 hours, until the system fully reacts, take the precipitates on both sides, wash and dry to obtain hydroxyapatite powder; The obtained hydroxyapatite powder 1g and 3mL complexed completely 0.15mol / LAgNO 3 After mixing, add ascorbic acid and transfer to a hydrothermal kettle. After 24 hours of hydrothermal heating, filter and wash the precipitate to obtain a hydroxyapatite / silver composite fungicide.
Embodiment 2
[0016] Measure 20mL 0.1mol / L CaSO 4 Aqueous solution, 20mL 0.06mol / L K 2 HPO 4 Add Triton-1000.02g to the aqueous solution, place the two solutions on both sides of the swim bladder, let stand for 10 hours, until the system fully reacts, take the precipitates on both sides, wash and dry to obtain hydroxyapatite powder; The obtained hydroxyapatite powder 1g and 2mL complexed completely 0.15mol / L AgNO 3 After mixing, add hydrazine hydrate and transfer to a hydrothermal kettle. After 24 hours of hydrothermal heating, filter and wash the precipitate to obtain a hydroxyapatite / silver composite fungicide.
Embodiment 3
[0018] Measure 20mL 0.1mol / L CaCl 2 Aqueous solution, 20mL 0.06mol / L NaH 2 PO 4 Add 0.02g of polyethylene glycol to the aqueous solution, put the two solutions on both sides of the egg membrane, let it stand for 10 hours, until the system fully reacts, take the precipitates on both sides, wash and dry to obtain hydroxyapatite powder ; The obtained hydroxyapatite powder 1g and 1mL complexed completely 0.15mol / LAgNO 3 After mixing, add glucose and transfer to a hydrothermal kettle. After 24 hours of hydrothermal heating, filter and wash the precipitate to obtain a hydroxyapatite / silver composite fungicide.
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