High-damping composition
A technology of high damping composition and basic polymer, which is applied in the direction of mechanical equipment, low internal friction springs, springs made of plastic materials, etc., can solve the problems of reduced processability of high damping compositions, blooming of high damping components, etc. The effect of achieving high damping performance
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Embodiment
[0111] Unless otherwise specified, the preparation and testing of the high damping composition in the following examples and comparative examples were carried out in an environment with a temperature of 20° C. and a relative humidity of 55%.
[0112]
[0113] 2 liters of distilled water was added to 150 ml of high-ammonia natural rubber latex [manufactured by SOTECH (Malaysia), rubber solid content concentration: 60.2% by mass], diluted so that the rubber solid content concentration became 10 mass%, and 0.12% naphthenic acid was added Sodium was used for stabilization, and then sodium dihydrogen phosphate was added to adjust the pH to 9.2.
[0114] Then, 7.8 g of alkaline protease [ALCALASE (registered trademark) 2.0M manufactured by Novozymes Japan Co., Ltd.] 2.0 M] was added as a deprotease and dispersed in 100 ml of distilled water, and the pH was adjusted to 9.2 again, and then the pH was adjusted at 37 The deproteinization treatment was carried out by keeping at ℃ for 2...
Embodiment 2
[0137] Except that the amount of alkaline protease as a deproteinase was 2.0 g, deproteinization treatment was performed in the same manner as in Example 1 to prepare a deproteinized natural rubber. The deproteinized natural rubber had a total nitrogen content of 0.25% by mass, a gel content of 18.8% by mass, and a weight average molecular weight of 1.3 million.
[0138] Furthermore, a high-damping composition was prepared in the same manner as in Example 1, except that the above-mentioned deproteinized natural rubber was used in the same amount.
Embodiment 3~5, comparative example 3、4
[0167] With respect to 100 parts by mass of deproteinized natural rubber as the base polymer, the amount of silica was 80 parts by mass (Comparative Example 3), 100 parts by mass (Example 3), 150 parts by mass (Example 4), Except 170 parts by mass (Example 5) and 180 parts by mass (Comparative Example 4), a high damping composition was prepared in the same manner as in Example 2.
[0168] The above-mentioned damping characteristic test was implemented on the high-damping composition prepared in each of the above-mentioned Examples and Comparative Examples, and their characteristics were evaluated. The results are shown in Table 3 together with the results of Example 2. In addition, all the resins in the characteristic column in a table|surface are the relative values when comparative example 1 was set as 100 as mentioned above.
[0169] table 3
[0170]
[0171] From the results of Examples 2 to 5 and Comparative Examples 3 and 4 in Table 3, it can be seen that by setti...
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