Extraction method of capsicum pigment
A capsaicin, extraction method technology, applied in chemical instruments and methods, azo dyes, organic dyes and other directions, can solve the problems of complex extraction process, easy to induce poisoning, can not be used as much or as little as possible, etc., achieve high nutritional value, convenient Simple operation and process
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Embodiment 1
[0014] Wash fresh red peppers and dry them in the sun. After separating the placenta and seeds, crush 10 kg of the obtained peels into a pulp, then place the pulpy pepper peels in a container, and add 2 times the volume of the pulp Heating to 55°C for n-hexane, heat preservation for 1 hour for extraction; stop heating, and filter after cooling to room temperature, continue to add n-hexane heating and extracting the filter residue according to the above method twice, filter after cooling, combine the filtrates and put them into distillation In the container, heat and distill under reduced pressure to recover n-hexane, and the residual liquid is oleoresin; add a 30% sodium hydroxide solution equal to the amount of oleoresin, heat to 70°C under constant stirring, and keep warm for 1 hour; After the mixed solution is lowered to room temperature, add hydrochloric acid dropwise under constant stirring until the pH value of the solution reaches 6 and stand for stratification. After th...
Embodiment 2
[0016] Wash fresh red peppers and dry them in the sun. After separating the placenta and seeds, crush 15 kg of the resulting peels into a slurry, then place the pulpy pepper peels in a container, and add 3 times the volume of the slurry For n-hexane, heat to 60°C, keep it warm for 1 hour to extract; stop heating, cool to room temperature and then filter, continue to add n-hexane to heat and extract the filter residue according to the above method, filter after cooling, combine the filtrates and put them into distillation In the container, heat and distill under reduced pressure to recover n-hexane, and the residual liquid is oleoresin; add a 40% sodium hydroxide solution equal to the amount of oleoresin, heat to 80°C under constant stirring, and keep warm for 1.5 hours; After the mixed solution was lowered to room temperature, hydrochloric acid was added dropwise under constant stirring until the pH value of the solution reached 7 and left to stand for stratification. After the...
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