Method for preparing pectin from capsicum residue
A technology of chili residue and pectin, applied in the field of preparation of pectin from chili residue, extraction and purification of chili residue pectin, can solve the problems of molecular chain break decolorization process, immature product quality, etc., achieve good decolorization effect and low cost Low, enhanced viscosity effect
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example 1
[0017] Take 1 kg of Jinta pepper, add 8 times the amount of boiling water, keep boiling for 10 minutes, filter, rinse the filter residue with warm water at about 50°C for 2-4 times, add 20 times the amount of 0.5% sodium hexametaphosphate acid water with a pH of 1.5, Stir slowly at 85°C for 3 times, each time for 2 hours, filter while hot, combine the filtrate, add 1% active carbon by weight of medicinal materials, stir, filter, concentrate the filtrate to 2500ml, add 5000ml of ethanol, stand still for 12 hours, filter, filter cake Elute 1000 ml with 60% ethanol, rinse once with 95% ethanol, dry the filter cake under reduced pressure (45°C), and grind to obtain 133.3 grams of milky white powder pectin. The yield was 13.33%.
example 2
[0019] Take 1 kg of Jinta pepper, add 8 times the amount of boiling water, keep boiling for 10 minutes, filter, rinse the filter residue with warm water at about 50°C for 2-4 times, add 15 times the amount of 0.5% sodium hexametaphosphate acid water with a pH of 1.9, Stir slowly at 85°C for 3 times, each time for 2 hours, filter while hot, combine the filtrate, add 1.5% active carbon by weight of medicinal materials, stir, filter, concentrate the filtrate to 3000ml, add 6000ml of ethanol, stand still for 12 hours, filter, filter cake Elute 1000 ml with 60% ethanol, rinse once with 95% ethanol, dry the filter cake under reduced pressure (45°C), and pulverize to obtain 142.3 grams of milky white powder pectin. The yield was 14.23%.
example 3
[0021] Take 1 kg of Jinta pepper, add 10 times the amount of boiling water, keep boiling for 10 minutes, filter, rinse the filter residue with warm water at about 50°C for 2-4 times, add 10 times the amount of 0.3% sodium hexametaphosphate acid water with a pH of 2.0, Stir slowly at 85°C for 3 times, each time for 3 hours, filter while hot, combine the filtrate, add 2% active carbon by weight of medicinal materials, stir, filter, concentrate the filtrate to 3000ml, add 6000ml of ethanol, stand still for 12 hours, filter, filter cake Elute 1000 ml with 60% ethanol, rinse once with 95% ethanol, freeze-dry, and pulverize to obtain 128.3 grams of milky white powder pectin. The yield was 12.83%.
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